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- 주제어 : curing rate test (검색결과 4 건)
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콘크리트포장 위 아스팔트 덧씌우기용 택코팅 재료의 접착강도특성 연구
조문진 한국도로학회 2013 한국도로학회논문집 Vol.15 No.4
PURPOSES: The performance of tack coat, commonly used for layer interface bonding, is affected by application rate and curing time. In this study, bonding strength tests were performed according to the application rate and curing time of asphalt emulsion. Based on finding from this study, optimum application rates and curing times are proposed. METHODS: In order to investigate bonding characteristic of asphalt emulsion, tests were performed on both asphalt concrete pavement and portland concrete pavement. Also, asphalt emulsions were tested at the application rate of 0, 0.2, 0.4, 0.6, and 0.8ℓ/m2 and at the curing time of 0, 0.5, 1, 2, and 24 hours. Pull-off test and shear bonding strength test, which commonly used for bonding strength measurement of asphalt emulsion, were adopted for this study. To assess field performance under different testing condition, asphalt emulsions were applied to inservice pavement. Throughout coefficient of determination analysis between material index properties from asphalt emulsion and mechanical response from bonding strength tests, performance correlativity was analyzed. RESULTS: Test results show that optimum application rate for asphalt overlay on asphalt concrete pavement (AOA) and asphalt overlay on concrete pavement (AOC) was 0.4~0.5ℓ/m2 and 0.3~0.5ℓ/m2, respectively. According to the curing time increment, tensile strength and shear strength of AOC were increased to 22~44% and 20~39%, respectively. AOA case also show strength increment in tensile strength (42%) and shear strength (9%). We tested the applicability of tack coat materials at the field sites, and our findings demonstrated that the bonding (for D and E) and rapid curing (for B, C, and D, E) performances were superior than others. Among material index properties, there was a high correlation between penetration ratio and bonding strength test result. CONCLUSIONS : Result show that interlayer bonding strength was affected by asphalt emulsion type, application rate and curing time. AOC required slightly higher application (0.1ℓ/m2) than AOA. Both AOA and AOC cases show higher strength at longer curing time. Up to 2hours of curing, rapid strength increments were observed, but strength increment ratio was decreased after 2hours of curing. From the observed correlation between penetration ratio and bonding strength, it is expected that penetration ratio can be used as one of important factors affecting bonding strength analysis.
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박창무 ( Chang Moo Park ),최성옥 ( Seung Ok Choi ),정노희 ( Noh Hee Jeong ) 한국유화학회 2010 한국응용과학기술학회지 Vol.27 No.4
Polyurethane adhesive is used in various fields as flexible packaging materials including a food packaging field. Therefore, the purpose of this study is synthesis of polyurethane adhesive which uses aliphatic isocyanate, and compares with aromatic isocyanate. The isocyanates for this test are toluene-2,4-diisocyanate(TDI), hexamethylene diisocyanate(HDI), 4,4-dicydohexyl ethane diisocyanate(H12MDI), and isophorone diisocyanate(IPDI). And. the effect of any other diisocyanate are evaluated by several methods as for curing rate test, accelerate weathering test, and peel strength test. The polyurethane adhesive using curing catalyst and HDI has adhesion strength of about 560 g/15 mm between aluminium foil and nylon, about 1,520 g/15 mm between nylon and CPP. Those parameters are similar to polyurethane adhesive with TDI. Also, in case of curing rate, those are similar to TDI type polyurethane adhesive. Moreover, data of ΔE as color variation by QUV tester is equal to 4.12, as 48% against those of TDI type.
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박창무(Park Chang Moo),최성옥(Choi Seung Ok),정노희(Jeong Noh Hee) 한국유화학회 2009 한국응용과학기술학회지 Vol.27 No.4
Polyurethane adhesive is used in various fields as flexible packaging materials including a food packaging field. Therefore, the purpose of this study is synthesis of polyurethane adhesive which uses aliphatic isocyanate, and compares with aromatic isocyanate. The isocyanates for this test are toluene-2,4-diisocyanate(TDI), hexamethylene diisocyanate(HDI), 4,4-dicyclohexyl ethane diisocyanate(H12MDI), and isophorone diisocyanate(IPDI). And, the effect of any other diisocyanate are evaluated by several methods as for curing rate test, accelerate weathering test, and peel strength test. The polyurethane adhesive using curing catalyst and HDI has adhesion strength of about 560 g/15 mm between aluminium foil and nylon, about 1,520 g/15 mm between nylon and CPP. Those parameters are similar to polyurethane adhesive with TDI. Also, in case of curing rate, those are similar to TDI type polyurethane adhesive. Moreover, data of △E as color variation by QUV tester is equal to 4.12, as 48% against those of TDI type.
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강길호 ( Kang Gil Ho ),최원종 ( Choe Won Jong ),박상윤 ( Park Sang Yun ) 한국복합재료학회 2003 Composites research Vol.16 No.6
복합재료의 열화에 의한 미세한 손상을 실제적으로 관찰하기는 쉽지 않다. 복합재료의 열화는 심각한 blistering이 일어나기 전에 chain scission, oxidation 등의 분자적인 상변화 과정을 거쳐 모재 또는 모재와 강화제 사이의 계면에서 미세한 delamination이 발생하고 성장한다. 복합재료의 열화에 의한 초기 열손상은 기계적인 특성에 큰 영향을 주게 된다. 본 연구에서는 복합재료 부품이 열이나 화염에 단기간 노출되었을 경우 및 경화도에 따른 초음파 투과특성을 분석하였다. 온도와 시간에 따라 열화시험을 실시하고 초음파 탐상을 통하여 absorption coefficient를 측정한 결과 열화에 의한 미소균열과 분자적인 상변화에 의하여 열화도가 높을수록 높은 absorption coefficient값을 보였다. 경화온도를 달리하여 경화된 복합재료의 초음파 탐상 결과 경화온도가 높을수록 absorption coefficient 값은 높아졌으며 material velocity는 낮아지는 경향을 보였다. 이는 높은 온도에서 경화될수록 수분 및 휘발성분에 의한 void와 같은 결함이 많이 발생하고 분자구조적인 측면에서 높은 온도에서 경화된 경우 초음파흡수율이 높은 망상구조가 형성되기 때문이다. The initial thermal degradation of polymer matrix composite is not observed easily. At the beginning of thermal degradation of polymer matrix composites, phase transformation such as chain scission, oxidation occur, and then micro delamination is produced in matrix and interface between matrix and fiber before blistering. Initial heat damage deteriorate mechanical properties of composites. We presented the detection method of the initial heat damage of composites conveniently using ultrasonic technique. Absorption coefficient and material velocity was measured with thermal degradation and degree of cure. The more thermal degradation was progressed, the more absorption coefficient was increased. When the cure temperature is more high, the absorption coefficient of cured composite is increased and material velocity is decreased. We concluded that cure temperature is more high, the defects such as void is increased and molecular structure cured at high temperature has cross-linking structure which is more absorb the ultrasonic waves.
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