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In situ growth of hollow Cu2O spheres using anionic vesicles as soft templates
Xiaolin Luo,Zhe Pan,Fei Pei,Zhipeng Jin,Kangkang Miao,Pengfei Yang,Huaming Qian,Qiang Chen,Guodong Feng 한국공업화학회 2018 Journal of Industrial and Engineering Chemistry Vol.59 No.-
Geometrically optimizing anionic vesicles were fabricated using two types of anionic surfactants with antipodal molecular configuration. The influence of counterions on the anionic vesicles was systematically investigated to maintain electrostatic interaction between the anionic vesicles and the precursors, as well as to ensure the structural integrity of the vesicle templates. The transcription from vesicles to hollow Cu2O spheres was achieved through an in situ reduction approach. The obtained hollow Cu2O spheres were assembled by abundant nanoparticles around the vesicle interface and showed preferable adsorption capacity for methyl orange in the dark compared with the solid Cu2O spheres synthesized without any surfactants.
Wu Jin,Lei Genping,Wang Ting,Dong Sheng,Zhan Xiaolin 대한독성 유전단백체 학회 2022 Molecular & cellular toxicology Vol.18 No.3
Background Membranous nephropathy is characterized by deposition of immune complex. The initial inflammatory responses induce cell apoptosis and oxidative injury, thus contributing to the pathogenesis of chronic kidney disease. Esculentoside A exerts anti-inflammatory, anti-apoptotic and anti-oxidant abilities, and protects against acute kidney injury. Objective The renoprotective effect of Esculentoside A on a rat model with membranous nephropathy was investigated in this study. Results Injection of cationic bovine serum albumin promoted the level of 24 h proteinuria, and induced histopathological damage, including glomerular atrophy and thick glomerular basement membrane in the kidney tissues. Intraperitoneal injection with Esculentoside A reduced the level of 24 h proteinuria, and attenuated the pathological damages. Esculentoside A attenuated cationic bovine serum albumin-induced reduction of Bcl-2 protein expression, enhancements in the protein expressions of Bax and cleaved caspase-3. Besides, the enhanced levels of MDA (malondialdehyde) and NO (nitric oxide), and reduced levels of SOD (superoxide dismutase) and GSH (glutathione), in rats with membranous nephropathy were restored by Esculentoside A injection. Moreover, Esculentoside A counteracted with the promotive effects of cationic bovine serum albumin on the protein expressions of phosphorylated JNK (p-JNK), p-ERK1/2 and p-p38. Conclusion The renoprotective effects of Esculentoside A on a rat model with membranous nephropathy was mediated by its anti-oxidant and anti-apoptotic effects through inactivation of MAPKs pathway.
Electric-Field-Assisted Assembly of Polymer-Tethered Gold Nanorods in Cylindrical Nanopores
Wang, Ke,Jin, Seon-Mi,Xu, Jiangping,Liang, Ruijing,Shezad, Khurram,Xue, Zhigang,Xie, Xiaolin,Lee, Eunji,Zhu, Jintao American Chemical Society 2016 ACS NANO Vol.10 No.5
<P>In this report, we demonstrate the confined assembly of polymer-tethered gold nanorods in anodic aluminum oxide (AAO) channels with the assistance of electric field (EF). Various interesting hybrid assemblies, such as single-, double-, triple-, or quadruple-helix, linear, and hexagonally packed structures are obtained by adjusting pore size in AAO channels, ligand length, and EF orientation. Correspondingly, surface plasmonic property of the assemblies can thus be tuned. This strategy, by coupling of external-field and cylindrically confined assembly, is believed to be a promising approach for generating ordered hybrid assemblies with hierarchical structures, which may find potential applications in photoelectric devices, biosensors, and data storage devices.</P>
Xinkun Wang,Runqiang Yang,Xiaolin Jin,Yulin Zhou,Yongbin Han,Zhenxin Gu 한국식품과학회 2015 Food Science and Biotechnology Vol.24 No.6
Phytic acid is involved in storage of phosphorus and minerals in soybeans. The effects of 6 basic plant hormones on phytic acid degradation were investigated. After 6 days of germination, phytic acid contents in soybean sprouts decreased by 70%, compared with day 0 soybeans. Zn and Fe bioavailability of 6-day-old germinating soybean both significantly increased (p<0.05), by contrast, Ca bioavailability decreased compared with controls. Phytic acid was detectable only in cotyledons of soybean sprouts during germination. In germinating soybeans, 39.19-45.85% and 54.15-60.81% of phytase existed in embryos and cotyledons, respectively. Unlike phytase, acid phosphatase was present mainly in cotyledons (92.57-97.51%). Among the 6 hormones, 50 mg/L indoleacetic acid (IAA) brought the highest degradation value to phytic acid content, meanwhile, Zn, Fe, and Ca bioavailability of IAA-treated soybeans were significantly (p<0.05) improved, compared with that of the control, respectively.
Multi-Residue Analysis of Fipronil and Its Metabolites in Eggs by SinChERS-Based UHPLC-MS/MS
Han, Keguang,Hua, Jin,Zhang, Qi,Gao, Yuanhui,Liu, Xiaolin,Cao, Jing,Huo, Nairui Korean Society for Food Science of Animal Resource 2021 한국축산식품학회지 Vol.41 No.1
A method for simultaneous detection of fipronil (F) and its metabolites fipronil desulfinyl (FD), fipronil sulfide (FS), fipronil sulfone (FSO) in chicken eggs was applied and validated. It includes single-step, cheap, effective, rugged, safe-based method (SinChERS) for sample preparation and ultra high performance liquid chromatography coupled with mass spectrometry (UHPLC-MS/MS) for chemical analysis. Results suggested that formic acid enhanced the recovery of 4 target residues and 1% supplementation to acetonitrile gained higher recoveries than that of 5%. SinChERS integrated extraction and clean-up steps into one, with shorter time (1.5 h) to operate and higher recoveries (97%-100%) than HLB, Envi-Carb-NH2 and quik-easy-cheap-effective-rugged-safe method (QuEChERS), and it consumed the smallest volume of extracting solvent (10 mL) as QuEChERS. Quantitative analyses using external standard method suggested the linear ranges of 4 target compounds were 1-20 ㎍/L with R2 >0.9947. The limit of detection (S/N>3) and quantification (S/N>10) were 0.3 ㎍/kg and 1 ㎍/kg. Recoveries ranged from 89.0% to 104.4%, and the relative standard deviations (n=6) at 1, 10, and 20 ㎍/kg were lower than 6.03%. Thirty batches of domestic eggs (500 g each) were detected by the established SinChERS-based UHPLC-MS/MS and no target residues were detected in all samples. The method developed in this study is a rapid, sensitive, accurate and economic way for multi-residue analysis of fipronil and its metabolites in eggs.
Xinkun Wang,Runqiang Yang,Xiaolin Jin,Zhijie Chen,Yulin Zhou,Zhenxin Gu 한국식품과학회 2015 Food Science and Biotechnology Vol.24 No.5
Phytase/phosphatase activities, the phytic acid content, and Zn, Fe, and Ca bioavailability values of 4-d-germinated soybeans and mung beans were investigated. Phytase and phosphatase activities of germinated soybeans and mung beans both increased, compared with raw beans. The phytic acid contents declined in germinated soybeans by 57.5% and in mung beans by 76.0%. Zn and Fe bioavailability values increased in germinated beans and Ca bioavailability decreased. For incubation, the highest bioavailability values of Zn, Fe, and Ca, respectively, were achieved using an exogenous phytase treatment in mung beans (47.6, 44.6, and 51.5%). Soybeans exhibited values of 64.7, 60.6, and 47.9%, respectively, after a combined treatment with endogenous and exogenous phytases. Germination improves Zn and Fe bioavailability values of beans by increasing enzyme activity, but is time-consuming. Incubation is more efficient for improvement of Zn, Fe, and Ca bioavailability values in a short period of time.
Flow between eccentric cylinders: a shear-extensional controllable flow
Guoqiang Tian,Mengmeng Wang,Xiaolin Wang,Gang Jin 한국유변학회 2016 Korea-Australia rheology journal Vol.28 No.2
In this work the non-Newtonian fluid between eccentric cylinders is simulated with finite element method. The flow in the annular gap between the eccentric rotating cylinders was found to be a shear-extensional controllable flow. The influence of rotating speed, eccentricity as well as the radius ratio on the extensional flow in the vicinity of the minimum gap between the inner and outer cylinder was quantitatively investigated. It was found that both the strengths of shear flow and extensional flow could be adjusted by changing the rotating speed. In respect to extensional flow, it was also observed that the eccentricity and radius ratio exert significant influences on the ratio of extensional flow. And it should be noted that the ratio of extensional flow in the mix flow could be increased when increasing the eccentricity and the ratio of shear flow in the mix flow could be increased when increasing the radius ratio.
Experimental study of the influence of sodium salts as additive to NOxOUT process
Zhaoping Zhong,Xiujin Liang,Baosheng Jin,Xiaolin Chen,Weiling Li,Hongge Wei,Houkun Guo 한국화학공학회 2010 Korean Journal of Chemical Engineering Vol.27 No.5
An experimental study of the SNCR process with urea as reducing agent and sodium salts as additive has been carried out, and detailed analysis of the reaction mechanism has been given here. In the temperature range of 800-975 oC, NO concentration decreases at first and then increases while the concentration of N2O increases at first and then decreases with the increasing of temperature, and the turning point is 900 oC. With increasing of normalized stoichiometric ratio of reduction nitrogen to NOx (NSR), NO removal efficiency increases, while the concentration of N2O also increases, which decreases overall NOx removal efficiency. With sodium salts as additive, the concentration of N2O decreases with increasing of sodium salts addition at all temperatures, while the concentration of NO decreases at first and then increases at low-temperature side of the temperature window and increases at high-temperature side with additional increasing, whose changing extent is smaller than N2O. Since sodium salts as additive can remove N2O effectively and have no large influence on the removal of NO, the effect of sodium salts as additive is the combined effect of the production of active radicals and the removal of HNCO produced by the decomposition of urea through neutralization reactions, which is more important. To achieve the same effect under each condition, the needed addition of NaOH and CH3COONa is less than that of Na2CO3 counting as Na atom. For the decomposition of CH3COONa can produce CH3COO, its addition can promote the reduction of NO more obviously at the lower temperature than Na2CO3 or NaOH. Overall NOx removal efficiency at 900 oC with NSR=1.5 had been improved from about 30% to 70.45% through the addition of sodium salts. Sodium salts as additive caused the flue gas to become alkaline gas, but it was not serious for sodium salts existing as NaNCO.