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Lee, Jaehong,Seo, Jungmok,Kim, Dayeong,Shin, Sera,Lee, Sanggeun,Mahata, Chandreswar,Lee, Hyo-Sung,Min, Byung-Wook,Lee, Taeyoon American Chemical Society 2014 ACS APPLIED MATERIALS & INTERFACES Vol.6 No.12
<P>The fabrication of well-ordered metal nanoparticle structures onto a desired substrate can be effectively applied to several applications. In this work, well-ordered Ag nanoparticle line arrays were printed on the desired substrate without the use of glue materials. The success of the method relies on the assembly of Ag nanoparticles on the anisotropic buckling templates and a special transfer process where a small amount of water rather than glue materials is employed. The anisotropic buckling templates can be made to have various wavelengths by changing the degree of prestrain in the fabrication step. Ag nanoparticles assembled in the trough of the templates via dip coating were successfully transferred to a flat substrate which has hydrophilic surface due to capillary forces of water. The widths of the fabricated Ag nanoparticle line arrays were modulated according to the wavelengths of the templates. As a potential application, the Ag nanoparticle line arrays were used as SERS substrates for various probing molecules, and an excellent surface-enhanced Raman spectroscopy (SERS) performance was achieved with a detection limit of 10<SUP>–12</SUP> M for Rhodamine 6G.</P><P><B>Graphic Abstract</B> <IMG SRC='http://pubs.acs.org/appl/literatum/publisher/achs/journals/content/aamick/2014/aamick.2014.6.issue-12/am5000382/production/images/medium/am-2014-000382_0007.gif'></P><P><A href='http://pubs.acs.org/doi/suppl/10.1021/am5000382'>ACS Electronic Supporting Info</A></P>
Lee, Eunsongyi,Lee, Jun Min,Koo, Ja Hoon,Lee, Wooyoung,Lee, Taeyoon Elsevier 2010 International journal of hydrogen energy Vol.35 No.13
<P><B>Abstract</B></P><P>We report the fabrication of a novel hydrogen sensor that utilizes the electrical resistance changes in the palladium thin films with nanometer thicknesses. The sensing mechanism is based on transitory absorption of hydrogen atoms into the palladium layer, which leads to the reversible alteration of the electrical resistance. In concentrated hydrogen ambient, the excess hydrogen absorption process leads to mechanical deformation on the surface of the palladium films, corresponding to the phase transition from α-phase to β-phase. The reversible sensing process results in a hysteresis curve for resistive properties, of which the height (sensitivity) could be controlled by manipulating the thickness of the palladium layers. The peel-off phenomena on the surface of the palladium film were suppressed by decreasing the thickness of the film. At the thickness of 20nm, a hysteresis curve of resistance was obtained without any structural change in the palladium thin film. These results provide a significant insight to the fundamental understanding of the relationship between the electrical sensitivity of pure Pd thin films and related structural deformation, which is essential to develop robust H-sensors with high sensibility.</P>
Single-Crystalline Silicon-Based Heterojunction Photodiode Arrays on Flexible Plastic Substrates
Sangwook Lee,Juree Hong,Ja Hoon Koo,Seulah Lee,Kwanghyun Lee,Seongil Im,Taeyoon Lee IEEE 2011 IEEE transactions on electron devices Vol.58 No.10
<P>A silicon-based photodiode array was fabricated on a flexible polyethylene terephthalate substrate using a transfer printing technique. A heterojunction structure composed of a 15-nm-thick highly doped hydrogenated amorphous-silicon (n<SUP>+</SUP> a-Si:H) layer and a 3-μm-thick p-type single-crystal silicon (p c-Si) membrane layer was adopted as the active layer of the flexible photodiode. The highly ordered photodiode array formed on the flexible substrate exhibited superior stability in electrical properties under bent conditions with no mechanical deformation. The variation of the spectral quantum efficiency (QE) under short-wavelength light illumination (λ ≤ 580 nm) was in excellent agreement with that of a heterojunction photodiode composed of a-Si:H and a bulk c-Si substrate. Relatively low QE values were observed under longer wavelength (λ ≥ 600 nm) illumination due to the finite thickness of the active layer. The <I>C</I>-<I>V</I> measurement results of the fabricated photodiode array were in accordance with the abrupt junction model. A closer inspection of the junction area of the device using high-resolution cross-sectional transmission micrograph exhibited an interface depth of 2 ± 0.5 nm, which is unavoidable in plasma-enhanced a-Si:H deposition processes.</P>
GC/FPD를 이용한 환경기초시설 폐기물의 대기중 황계열 악취물질 배출특성에 관한 연구
이태윤(Lee Taeyoon),이제근(Lee Jeakeun),이준기(Lee Junki) 한국지반환경공학회 2009 한국지반환경공학회논문집 Vol.10 No.2
우리나라는 경제발전과 더불어 하수종말처리장과 음식물쓰레기처리시설의 수가 꾸준히 증가해왔다. 이들 시설들은 상수원 수질보전과 음식물쓰레기 재활용과 같은 긍정적인 역할을 수행하지만 한편으로는 심각한 악취문제를 유발해 인근주민들의 쾌적한 생활을 해치고 있는 실정이다. 이에 본 연구에서는 부산시 환경기초시설에서 발생되고 있는 탈수슬러지케잌 및 음식물쓰레기 샘플을 채취, 황화수소 발생 가능량을 예측함과 동시에 발생 가능량이 많을 것으로 나타난 1개 시료를 선정하여 실험실 규모의 Flux Chamber 실험을 통해 대기 시료를 포집하여 GC/FPD분석을 실시, 혐기성 상태일 때 이들 처리장폐기물에서 대기 중으로 배출하는 황계열 악취물질에 대한 배출농도 측정결과를 제시하고자 하였다. 황화수소발생량이 가장 많은 시료는 녹산 하수처리장의 슬러지 샘플로 농도가 156.18㎎/㎏이었고, GC/FPD로 분석을 실시한 결과를 토대로 악취농도지수(Odor Quotient)를 산정해 본 결과 개별 악취물질중 CH₃SH(methylmercaptan)이 총악취농도지수에서 차지하는 비율이 47.3%로 가장 주요 악취원인물질로 나타났다. With the economic development of Korea, sewage treatment facilities and waste food treatment facilities have been steadily increased. These facilities have positive effects such as the conservation of the water resources quality and waste food recycling while they also affect the neighborhood life with severe odor problems. Therefore, it was first collected sludge samples from 5 sewage treatment facilities and 5 waste food treatment facilities where the amounts of waste produced from above sites are relatively immense in Busan and estimate the H₂S emission rates. Then it was selected 1 sample which has the highest emission rate of H₂S. Using flux chamber and GC/FPD analyses, it was tried to quantify the emitted amount of sulfonic gas concentration under anoxic condition. The sludge sample obtained from Noksan sewage treatment facility has the highest emission rate of H₂S. This sample contained 156.18 ㎎/㎏ H₂S. The odor compounds were analyzed using GC/FPD and the concentrations were converted to odor quotient. Among odor compounds the ratio of CH₃SH (methylmercaptan) for the total odor quotient was 47.3% and considered to be the main odor compound in the sample.
Lee, Jaehong,Shin, Sera,Lee, Sanggeun,Song, Jaekang,Kang, Subin,Han, Heetak,Kim, SeulGee,Kim, Seunghoe,Seo, Jungmok,Kim, DaeEun,Lee, Taeyoon American Chemical Society 2018 ACS NANO Vol.12 No.5
<P>Highly stretchable fiber strain sensors are one of the most important components for various applications in wearable electronics, electronic textiles, and biomedical electronics. Herein, we present a facile approach for fabricating highly stretchable and sensitive fiber strain sensors by embedding Ag nanoparticles into a stretchable fiber with a multifilament structure. The multifilament structure and Ag-rich shells of the fiber strain sensor enable the sensor to simultaneously achieve both a high sensitivity and largely wide sensing range despite its simple fabrication process and components. The fiber strain sensor simultaneously exhibits ultrahigh gauge factors (∼9.3 × 10<SUP>5</SUP> and ∼659 in the first stretching and subsequent stretching, respectively), a very broad strain-sensing range (450 and 200% for the first and subsequent stretching, respectively), and high durability for more than 10 000 stretching cycles. The fiber strain sensors can also be readily integrated into a glove to control a hand robot and effectively applied to monitor the large volume expansion of a balloon and a pig bladder for an artificial bladder system, thereby demonstrating the potential of the fiber strain sensors as candidates for electronic textiles, wearable electronics, and biomedical engineering.</P> [FIG OMISSION]</BR>