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Saleem M.,Naz M.Y.,Shukrullah S.,Farooq M.U.,Zahid M.,Hussain Z.,Makhlouf M.M. 한국물리학회 2021 Current Applied Physics Vol.31 No.-
A single step ultrasonic biosynthesis method was used to synthesize and coat TiO2 nanoparticles onto DBD plasma functionalized raw cotton. Titanium isopropoxide was reduced with aloe vera plant extract into TiO2 nanoparticles. The effect of DBD plasma treatment on self-cleaning property of TiO2 coated fabric was optimized statistically by using a complete composite design. To induce functional groups on the cotton fabric surface, the fabric was pre-treated with DBD plasma over various periods of time. The plasma exposure time, molarity of solution and ultrasonication time were optimized using complete composite design package. TiO2 nanoparticles revealed spherical shape and anatase phase with average crystallite size of 10.46 nm. The statistically optimized plasma exposure time, molarity and sonication time was 7 min, 0.80 and 75 min, respectively. The plasma activation of fabric significantly improved the adsorption, tensile strength and self-cleaning ability of TiO2 coated fabric.
Saleem M.,Naz M.Y.,Shukrullah S.,Shujah M. A.,Akhtar M.,Ullah Sami,Ali S. 한국탄소학회 2022 Carbon Letters Vol.32 No.1
The carbon-based nanostructures are in limelight due to their widespread applications in nano-to-micro-scale technologies. The carbon dots are known for their unique physical, electrical, optical, chemical and biological properties. The carbon dots (CDs) are being produced through several well-developed synthesis methods, one of which is the green sonochemical. This method is preferred over others because it is a green source of energy, facile, fast, low-temperature process, non-toxic and less expensive. Despite the fact of using 90% less energy than other methods, this method has been overlooked in the published literature. It is possible to prepare pure and doped CDs of low toxicity and controlled physicochemical properties through sonochemical method. In recent years, sonochemically produced CDs have been tuned and characterized for a variety of applications. This review has explored the merits and demerits of sonochemical method in comparison to the other methods for the synthesis of pure CDs and their nanocomposites. The role of multiple factors in tailoring the specific parameters of CDs for their application in antibacterial, polymerization, tissue engineering, catalysis, bio-imagining, supercapacitors, drug delivery and electric devices is also elaborated in this review. This review also concludes on future directions in the applications of sonochemically produced CDs.