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안세진,SHANMUGAMMANIVANNAN,서예지,김규원 대한화학회 2019 Bulletin of the Korean Chemical Society Vol.40 No.6
Electrochemically deposited standing platinum (Pt) nanoplates were fabricated on gold (Au) substrate assisted by the amine functionalized silane and L-glutamic acid (LG) as nucleating and structure directing agents, respectively. Various win over factors responsible for the electrodeposition of the Pt nanoplates was methodologically analyzed. The treatment time with the thiol functionalized silane (M) and the role of LG were found to be decisive for the demonstration of Pt nanoplates display at the Au substrate. Plausible growth mechanism was proposed for the vertical growth and random orientation of the Pt nanoplates. Constructed Pt nanoplates displayed substrate were applied as a sensor platform toward the nitrite ion detection; improved performance was noted than that of the controlled experiments. Furthermore, sensor platform had exhibited recent selectivity toward the nitrite ions from the mixture of possible interferences.
Petal-like MoS2 nanostructures with metallic 1 T phase for high performance supercapacitors
Rajneesh Kumar Mishra,SHANMUGAMMANIVANNAN,김규원,권혁인,진성훈 한국물리학회 2018 Current Applied Physics Vol.18 No.3
Herein, we report the metallic 1 T phase MoS2 petal-like nanostructures (MP-LNs), synthesized by the solvothermal method, for applications in supercapacitor electrodes. X-ray photoelectron spectroscopy (XPS) verified the composition and distribution of Mo and S, illustrating that the 1 T metallic phase is predominant in the MP-LNs. Electrochemical analyses were performed to explore the supercapacitor applications of the MP-LN material, demonstrating a superior cyclic voltammetry (CV), high specific capacitance, good stability. MP-LN-based supercapacitors (MP-LNS) show high specific capacitances of 811 F/g and 400 F/g at current densities of 0.1 A/g and 10 A/g, respectively. The long-term cycling stability was also studied to investigate the reproducible nature of MP-LNS and was found to display excellent specific capacitance retention of 49.3% (at 0.1 A/g) and 82.7% (at 10 A/g) after 1000 charge-discharge cycles, which indicates good reversibility of the galvanostatic charge-discharge (GCD) of the electrode material. These findings highlight the potential use of MP-LNs in supercapacitors.