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        Influence of Iron Doping on Structural, Optical and Magnetic Properties of TiO2 Nanoparticles

        R. Zahid,M. Manzoor,A. Rafi q,M. Ikram,M. Nafees,A. R. Butt,S. G. Hussain,S. Ali 대한금속·재료학회 2018 ELECTRONIC MATERIALS LETTERS Vol.14 No.5

        In this study, various concentrations of Fe doped TiO2nanoparticles have been successfully synthesized using the sol–gelmethod. A variety of characterization techniques as ultra-violet visible (UV–Vis) spectroscopy, X-ray diffractometer (XRD),vibrating sample magnetometry (VSM) and field emission scanning electron microscopy (FESEM) were employed to analyzethe prepared nanopowders. XRD measurement confirmed the substitution of Fe ion without disturbing the tetragonal crystalsystem of TiO2. The crystallite size was found to decrease and lattice strain increases upon doping estimated by WilliamsonHall plot. Furthermore, the average grain size calculated by FESEM found was between 10 and 30 nm for pure and dopedTiO2. UV–Vis spectroscopy showed an increase in absorption accompanied red shift and increase in band gap energies from3.36 to 3.62 eV with the addition of Fe. The FTIR spectroscopy was employed to confirm the presence of functional groupsin the fabricated nanopowders. Upon mixing the saturation magnetization (Ms) varying from (2.12 to 1.51)10−2 emu/g wasobserved.

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        Effect of Season and Age on the Ovarian Size and Activity of One-Humped Camel (Camelus dromedarius)

        Ali, Shujait,Ahmad, Nazir,Akhtar, Nafees,Rahman, Zia-ur,Sarwar, M. Asian Australasian Association of Animal Productio 2007 Animal Bioscience Vol.20 No.9

        In this project, ovarian size and activity during the peak (November-April) and the low (May-October) breeding seasons in young and adult camels were studied. Ovaries of 92 camels (Camelus dromedarius), with clinically normal reproductive tracts, aged 3-15 years and slaughtered at Faisalabad or Lahore abattoirs over a period of 24 months, were collected. Jugular blood was collected from each animal before slaughter; the serum was separated and analyzed for oestradiol concentration. The size (length, width and thickness) and weight of each ovary were measured. Grossly observable Graafian follicles were counted and their diameter was measured using Vernier Calipers. The camels having ovaries presenting follicles more than 5 mm in diameter were taken as having active ovaries. The results showed that ovarian length, width and weight were significantly higher (p<0.05) during the peak than the low breeding season. The percentage of active ovaries was also significantly higher (p<0.01) during the peak than the low breeding season. However, the effect of season on ovarian thickness was non-significant. Similarly, the ovarian length, width, thickness, weight and activity did not vary significantly between young (3-7 years old) and adult (8-15 years old) animals. Serum oestradiol concentrations were significantly higher (p<0.05) during the peak ($67.70{\pm}1.36$ pg/ml) than the low breeding season ($15.25{\pm}1.54$ pg/ml). It was concluded that in Pakistani camels ovarian size and activity were higher during the peak than the low breeding season. However, age of the camel (from 3 to 15 years) had no effect on these parameters.

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