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Kinetics and optimization of L-tryptophan separation with ion-exchange chromatography
Wei Luo,Limei Fan,Peilian Wei,Hao Chen,Limei Fang,Jin Huang,Zhinan Xu,Peilin Cen 한국화학공학회 2011 Korean Journal of Chemical Engineering Vol.28 No.5
Adsorption and desorption of L-tryptophan (L-trp) on strong acid cation exchange resin were investigated in a fixed-bed column. L-trp was effectively adsorbed onto the resin HZ-001, with the loading capacity and breakthrough time determined. Four kinetic models, including Adams-Bohard, Wolborska, Thomas, and Yoon-Nelson models,were adopted to determine the kinetic parameters of adsorption and to predict the breakthrough curves. The results showed that the models used described the breakthrough well. Desorption of L-trp from the column bed was performed using aqueous ammonia as the eluant. Optimum procedure was obtained with 2.0M aqueous ammonia at the elution velocity of 6 BV/h. Five cycles of adsorption-elution-regeneration were conducted to evaluate the column reutilization.
Xu Zhang,Zeyong Wei,Yuancheng Fan,Limei Qi 한국물리학회 2017 Current Applied Physics Vol.17 No.6
A reflective metamaterial polarization transformer (RMPT) is proposed with closed fish-scale structure for high efficient cross-polarization reflection. The maximum efficiency of cross-polarization reflection for normal incidence is 97.2%. The RMPT maintains good performance for incident angles up to 25, and the RMPT is not restricted to a specific polarization state of the incident wave. Furthermore, the designed RMPT shows excellent structural tunability by optimizing the structural parameters, which makes it userfriendly.