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Jiasheng Lin,Shuliang Yang,Yanjie Wang,Yahan Cui,Qiaoyan Li,Yanhua Chen,Lan Ding 한국공업화학회 2022 Journal of Industrial and Engineering Chemistry Vol.114 No.-
A novel type of biomass carbonized polymer dots (CS-CPDs) with green fluorescence emission were synthesizedvia a one-step microwave-assisted method, using chitosan and maleic acid as the precursors. The fluorescence intensity of CS-CPDs was selectively enhanced (turn on) with increasing levofloxacin(LEV) concentration based on Aggregation Induced Emission Enhancement. The linear range of thismethod was 1–35 lmol/L, with the limit of detection of 0.20 lmol/L. Furthermore, we demonstrated thatthe fluorescence intensity of CS-CPDs/LEV was restored (turn on-off) due to the addition of copper (II),which could assemble a more stable Cu2+/LEV complex through coordination. For the first time, CSCPDswere utilized as a selective fluorescent ‘‘turn on-off” probe for the continuous detection of LEVand Cu2+. Excellent results were also obtained in environmental water samples analysis with recoveriesranging of 91.3–99.6% and 97.7–113.4%, respectively. Moreover, the prepared CS-CPDs exhibited excellentoptical stability and large Stokes shift (139 nm), which predicted broad application prospects inthe field of fluorescence sensing.
Xu, Jiasheng,Sun, Yudong,Lu, Mingjun,Wang, Lin,Zhang, Jie,Qian, Jianhua,Kim, Eui Jung ELSEVIER SCIENCE 2017 JOURNAL OF ALLOYS AND COMPOUNDS Vol.717 No.-
<P><B>Abstract</B></P> <P>Porous Mn<SUB>2</SUB>O<SUB>3</SUB> microsheet arrays on nickel foam have been prepared by a mild chemical reaction combined with a calcination process. The porous Mn<SUB>2</SUB>O<SUB>3</SUB> microsheet arrays are directly grown on the surface of the conductive nickel foam. The porous Mn<SUB>2</SUB>O<SUB>3</SUB> microsheet arrays are composed of numerous interconnected nanopores with an average size of about 16 nm. The specific surface area of the porous Mn<SUB>2</SUB>O<SUB>3</SUB> materials is 36.34 m<SUP>2</SUP> g<SUP>−1</SUP>. The fabricated electrode materials exhibit a high specific capacitance of 566.6 F g<SUP>−1</SUP> at a current density of 0.5 A g<SUP>−1</SUP> and 294.4 F g<SUP>−1</SUP> at a current density of 20 A g<SUP>−1</SUP>. The energy density of the porous Mn<SUB>2</SUB>O<SUB>3</SUB> microsheet was 19.65 Wh kg<SUP>−1</SUP> at a power density of 124.85 W kg<SUP>−1</SUP> and it was reduced to 10.22 Wh kg<SUP>−1</SUP> at a power of density of 5.00 kW kg<SUP>−1</SUP>. The good electrochemical capacitance is ascribed to the interconnected porous structure of the Mn<SUB>2</SUB>O<SUB>3</SUB> microsheet, which facilitates electrolyte diffusion and enhances electron transport. The porous Mn<SUB>2</SUB>O<SUB>3</SUB> microsheet arrays on nickel foam are a promising electrode material for supercapacitors.</P> <P><B>Highlights</B></P> <P> <UL> <LI> Porous Mn<SUB>2</SUB>O<SUB>3</SUB> microsheet arrays on nickel foam are synthesized via solution process followed with an annealing treatment. </LI> <LI> It directly utilizes as electrode materials for pseudocapacitors. </LI> <LI> A specific capacitance of 566.6 F g<SUP>−1</SUP> is achieved at a current density of 0.5 A g<SUP>−1</SUP>. </LI> </UL> </P> <P><B>Graphical abstract</B></P> <P>[DISPLAY OMISSION]</P>
Qiaoyan Li,Yahan Cui,Jiasheng Lin,Chun Zhao,Lan Ding 한국공업화학회 2022 Journal of Industrial and Engineering Chemistry Vol.110 No.-
In this paper, the snowflake-like ZnO nanomaterials were prepared by combining zinc salt impregnationand high-temperature calcination with carbon microspheres as the sacrificial template. The effects ofethanol concentration in aqueous solution on the microstructure and sensing properties of ZnO nanomaterialswere investigated. The results showed that using 25 % ethanol-containing aqueous solution asimpregnation solution, snowflake-like ZnO nanomaterials (ZnO-25) showed excellent sensing performancefor NO2 at room temperature. It is mainly attributable to the rich channels and large specific surfacearea of the snowflake-like ZnO, which facilitates the rapid diffusion of the target gas. A large amountof chemisorbed oxygen can promote the surface reaction. In addition, the unremoved carbon during calcinationpromotes the electrical properties of ZnO. This strategy will provide a new sight on developing atype of sensitive NO2 gas sensing device working at room temperature.
Junjie Shu,Ru Xia,Jiasheng Qian,JIBIN MIAO,LIFEN SU,Ming Cao,Hongyun Lin,Peng Chen,Jinyang Chen 한국고분자학회 2016 Macromolecular Research Vol.24 No.7
The composites of chlorinated polyethylene rubber (CM) filled with boron nitride (BN) were prepared and examined systematically. Scanning electron microscopy (SEM) was used to observe microscopic morphology of composites. Mechanical properties of composites were analyzed by a rubber process analyzer (RPA) and dynamic mechanical thermal analyzer (DMTA). Thermal conductivity as well as thermo stability of composites was improved by adding BN particles into the CM rubber. It was found that BN particles can reinforce the rubber matrix while they also break down the network of polymer chains and ruin the physical properties of the rubber matrix. During the dynamic compressing process, BN particles can transfer heat from the matrix and alleviate the heat build-up phenomenon. The BN/CM composites (volume content CBN=18%) with thermal conductivity 1.179 W/(m·K) and good flexibility (Elongation at break=320%) were prepared, which may be used as thermal interface materials in a dynamic compressing process.
A Phase-shifting Control IPOS High-voltage Generator with Low Output Voltage Ripple for X-Ray
Hongyu Feng,Hongyi Lin,Jiasheng Xu,Liang Wu,Guozhu Chen 전력전자학회 2023 ICPE(ISPE)논문집 Vol.2023 No.-
A high-voltage (HV) generator with phase-shifting closed-loop control for X-ray is proposed. The LCC topology with input parallel output series (IPOS) is used in the circuit, and the phase-shifting closed-loop control is adopted to reduce the output voltage ripple further. In this paper, the LCC resonant converter is modeled based on fundamental harmonic approximation (FHA), and the output voltage ripple of a single module transformer is derived. On this basis, the output ripple of the multi-module LCC cascade converter is calculated and analyzed. Aiming at the problem that the ripple cancellation effect deteriorates due to the inconsistent parameters between modules, a phase locked loop (PLL) phase-shifting closed-loop control strategy is proposed. The simulation and experiment results show that the control method is feasible and reasonable.