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RISS 인기검색어
- 검색키워드
- 저자 : Chaoqian Lou (검색결과 2 건)
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Modification of Wool via Grafting β-cyclodextrin Oxidized by Sodium Periodate
Chaoqian Lou,Yuanyuan Yin,Xiuzhi Tian,Haibo Deng,Yingxia Wang,Xue Jiang 한국섬유공학회 2020 Fibers and polymers Vol.21 No.8
The modification of wool fabrics is significant in preparation of functional textiles. Sodium periodate oxidized β-cyclodextrin was grafted onto wool fabric through Schiff base reaction to obtain fabric with controlled release property. β-cyclodextrin was oxidized to aldehyde-β-cyclodextrin, and the results show that the inclusion constant and aldehyde contentof aldehyde-β-cyclodextrin are varied with the reaction parameters such as molar ratio of reaction agents and the reactiontemperature. The degree of oxidation was confirmed by ion chromatography. The drug loading test shows that the oxidizedcyclodextrin still had inclusion ability towards phenolphthalein, while the inclusion constant was only 50 % of the original β-CD. The ATR-FTIR spectra proved the occurrence of grafting reaction between the aldehyde groups of aldehyde-β-cyclodextrin and the amino groups on wool fiber. The aldehyde-β-cyclodextrin grafted wool fabric show great washingdurability even after 5 washing cycles. Compared with the aldehyde-β-cyclodextrin power, the inclusion ability of aldehyde-β-cyclodextrin fixed on the wool fiber decreased by 60 %.
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Chaoqian Lou,Yuanyuan Yin,Xiuzhi Tian,Haibo Deng,Yingxia Wang,Xue Jiang 한국섬유공학회 2020 Fibers and polymers Vol.21 No.1
β-cyclodextrin (β-CD) was oxidized by sodium periodate to yield a mixture of dialdehyde oligosaccharides. Theperiodate-oxidized β-CD (O-β-CD) together with chitosan (CTS) was firstly used to finish poly(ethylene terephthalate)(PET) fabrics by immersion-padding method, in which O-β-CD acted as a hydrophilic finishing agent plus a cross-linker. Theprocesses including the periodate oxidization of β-CD and the CTS/O-β-CD hydrophilic finishing of PET fabrics were ecofriendly. The results from the hydroxylamine hydrochloride titration showed that the aldehyde content in O-β-CD was3.0 mmol/g. With increasing the CTS/O-β-CD mass ratio, the finished fabric had better hydrophilic properties. When theCTS/O-β-CD mass ratio was 1:1, the moisture regain and water drops wetting time of the finished fabric reached 1.85 % and5.06 s, respectively. They became 1.50 % and 5.70 s, respectively after 25 times of laundering cycle. The occurrence of crosslinkingbetween O-β-CD and CTS was confirmed by the gel test and FT-IR characterization. The cross-linking networkdeposited on the fiber surface brought on excellent wash resistance of the CTS/O-β-CD finished PET fabrics.
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