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Manli Li,Enqi Jin,Zhiyong Qiao,Yuting Xiong 한국섬유공학회 2019 Fibers and polymers Vol.20 No.9
In order to study the effects of molecular structure of carboxyl-containing vinyl monomers on applicationperformance of feather keratin (FK) graft copolymer for warp sizing, three kinds of carboxyl acids, i.e. acrylic acid (AA),methacrylic acid (MAA), and itaconic acid (IA), were grafted onto molecular chains of FK through initiation of K2S2O8-NaHSO3 redox system. FK-g-PAA, FK-g-PMAA, and FK-g-PIA with similar grafting ratios around 31 % were prepared assizing agents. Major sizing properties of the three grafted keratins were studied in terms of water-solubility, apparentviscosity, contact angles of sizing paste on cotton fibers, mechanical properties of sizing film, and adhesion to fibers. It wasfound that sizing properties of the grafted FK strongly depended on molecular structure of the carboxyl-containing vinylmonomers. In view of overall performance of the grafted keratin sizes, the most appropriate carboxyl-containing vinylmonomer should be AA.
Li Tingting,Cao Shunwang,Wang Yi,Xiong Yujuan,He Yuting,Ke Peifeng,Huang Xianzhang 대한진단검사의학회 2021 Annals of Laboratory Medicine Vol.41 No.1
Background: A small shift in high-sensitivity cardiac troponin T (hs-cTnT) assays can lead to different result interpretation and consequent patient management. We explored whether a small bias could be detected using conventional internal quality control (QC) procedures, evaluated the performance of moving average (MA)-based QC procedures, and proposed a new QC procedure based on the moving rate (MR) of positive patient results of hs-cTnT assays. Methods:The ability of conventional QC to detect a 5 ng/L bias was examined using the13s/ 22s/R4s multi-rule procedure as deviation rules.We developed MA and MR procedures for the hs-cTnT assay using eight months of patient data. The performance of different MA or MR procedures was investigated by calculating the median number of patient samples affected until a bias introduced into the dataset was detected (MNPed). After comparing the MNPed across different procedures, we selected an optimal MA or MR procedure for validation. Validation graphs were plotted using the minimum, median, and maximum number of results affected until bias detection. Results: Our conventional QC procedures could not detect a positive bias of 5 ng/L. When a positive bias was introduced, MNPed was much higher using MA than using MR, with cut-off values of 5 ng/L and 14 ng/L, respectively. MR validation charts for optimal procedures provided insight into the MR performance. Conclusions: The MR procedure could detect different errors with few false alarms. In the hs-cTnT assay, the MR procedure with a smaller cut-off value outperformed MA and conventional QC procedures for small bias detection.