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RISS 인기검색어
- 검색키워드
- 저자 : Sweta Rana (검색결과 3 건)
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Mudila, Harish,Joshi, Varsha,Rana, Sweta,Zaidi, Mohmd. Ghulam Haider,Alam, Sarfaraz 한국탄소학회 2014 Carbon Letters Vol.15 No.3
An attempt was made to investigate the effect of the preparation temperature on the electro-capacitive performance of polypyrrole (PPY)/graphene oxide (GO) nanocomposites (PNCs). For this purpose, a series of PNCs were prepared at various temperatures by the cetyltrimeth-ylammonium bromide-assisted dilute-solution polymerization of pyrrole in presence of GO (wt%) ranging from 1.0 to 4.0 with ferric chloride as an oxidant. The formation of the PNCs was ascertained through Fourier-transform infrared spectrometry, X-ray diffraction spectra, scanning electron microscopy and simultaneous thermogravimetric-differential scanning calorimetry. The electrocapacitive performance of the electrodes derived from sulphonated polysulphone-bound PNCs was evaluated through cyclic voltammetry with reference to Ag/AgCl at a scan rate (V/s) ranging from 0.2 and 0.001 in potassium hydroxide (1.0 M). The incorporation of GO into the PPY matrix at a reduced temperature has a pronounced effect on the electrocapacitive performance of PNCs. Under identical scan rates (0.001 V/s), PNCs prepared at 10 ± 1ºC render improved specificconductivity (526.33 F/g) and power density (731.19 W/Kg) values compared to those prepared at 30 ± 1ºC (217.69 F/g, 279.43 W/Kg). PNCs prepared at 10 ± 1ºC rendered a capacitive retention rate of ~96% during the first500 cycles. This indicates the excellent cyclic stability of the PNCs prepared at reduced tempera-tures for supercapacitor applications.
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Electrochemical oxidation-reduction and determination of urea at enzyme free PPY-GO electrode
Harish Mudila,Parteek Prasher,Sweta Rana,Beena Khati,M.G.H. Zaidi 한국탄소학회 2018 Carbon Letters Vol.26 No.-
This manuscript explains the effective determination of urea by redox cyclic voltammetric analysis, for which a modified polypyrrole-graphene oxide (PPY-GO, GO 20% w/w of PPY) nanocomposite electrode was developed. Cyclic voltammetry measurements revealed an effective electron transfer in 0.1 M KOH electrolytic solution in the potential window range of 0 to 0.6 V. This PPY-GO modified electrode exhibited a moderate electrocatalytic effect towards urea oxidation, thereby allowing its determination in an electrolytic solution. The linear dependence of the current vs. urea concentration was reached using square-wave voltammetry in the concentration range of urea between 0.5 to 3.0 μM with a relatively low limit of detection of 0.27 μM. The scanning electron microscopy was used to characterize the morphologies and properties of the nanocomposite layer, along with Fourier transform infrared spectroscopy. The results indicated that the nanocomposite film modified electrode exhibited a synergistic effect, including high conductivity, a fast electron-transfer rate, and an inherent catalytic ability.
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Harish Mudila,M.G.H. Zaidi,Sweta Rana,S. Alam 한국탄소학회 2016 Carbon Letters Vol.18 No.-
Sulphonated polysulphone (SPS) has been synthesized and subsequently applied as binder for graphene oxide (GO)-based electrodes for development of electrochemical supercapacitors. Electrochemical performance of the electrode was investigated using cyclic voltammetry in 1M Na2SO4 and 1M KOH solution. The fabricated supercapacitors gave a specific capacitance of 161.6 and 216.8 F/g with 215.4 W/kg and 450 W/kg of power density, in 1M Na2SO4 and 1M KOH solutions, respectively. This suggests that KOH is a better electrolyte than Na2SO4 for studying the electrochemical behavior of electroactive material, and also suggests SPS is a good binder for fabrication of a GO based electrode.
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