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산소와 구리의 공정반응에 의한 구리와 알루미나의 직접접합
이임렬,유환성 단국대학교 신소재기술연구소 1991 신소재 Vol.1 No.-
본 연구에서는 구리표면의 구리-산소간의 공정반응에 의하여 형성된 Cu-Cu_2O 공용액상 피막으로 고체 Cu금속과 Al_2O_3세라믹을 압력없이 직접접합시키는 방법을 조사하였으며 접합조건에 따른 접합특성, 파면 및 계면분석을 SEM, EDS, XRD 및 peeling 시험을 통하여 분석하였다. 1.5×10^-1 torr 진공하에서 1015℃의 온도에서 산화시킨 구리시편은 미세한 산화물 Cu_2O가 표면에 잘 형성되었다. 그후 공정온도 1065℃ 이상의 접합온도 1075℃에서 5분간 10^-3 torr의 진공하에서 직접접합시킨 시편은 접합력이 우수한 Cu/Al_2O_3 접합이 되었으며 접합후 구리기니 내에는 Cu2O가 석출된 공융조직을 갖고 있었다. 3분 산화조건에서 충분한 액상이 형성되어 29kg의 최대 접합강도를 보였으며 산회시간이 이보다 짧거나 불충분한 액상의 형성이나 산화물내의 균열 등으로 결합력이 저하하였다. 파단후 Al_2O_3 표면에는 Cu_2O nodule이 존재하였고 Cu족에는 nodule이 빠진홈을 관찰할 수 있었는바 cu2O/Al_2O_3계면 접착력은 Cu.Cu_2O계면보다 강함을 알 수 있었다. 또한 파단면에는 반응 생성물 CuAlO_2가 접합중 형성되었으나 이 반응층 두께는 SEM분해능 이하인 매우 얇은 것으로 생각된다. The direct bonding between Cu and Al_2O_3, utilizing Cu-Cu_2O skin melt formed on Cu surface by eutectic reation of Cu-O, is investigated in this study. The bond strength, fracture surface and interface structure with bonding conditions have been studied using SEM, EDS, XRD and peeling test. A fine Cu_2O is formed on the surface of Cu with oxidation at 1015℃ under 1.5×10^-1torr vacuum. After oxidation, the bonded specimen conducted at 1075℃ in 10^-3torr vacuum for 5minutes, higher temperature than its eutectic temperature of 1065℃, has a good strength having a Cu_2O precipitated structure in Cu matrix upon cooling. It has been found that the maximum bonding force of 29kg is obtatined for 3 minutes of oxidation. However, the adhesion forces are decreased with shorter or longer oxidation than this due to the formation of insufficient liquid skin or crack within oxide. After peeling test, Al_2O_3 surface is covered with Cu_2O nodules which are pulled out of Cu surface indication that Cu_2O/Al_2O_3 adhesion force is stronger than that of Cu/Cu_2O. Moreover a reaction phase of CuAlO_2, thought to be very thin layer below the resolution of SEM, is also formed during the bonding process.
李任烈 단국대학교 1986 論文集 Vol.20 No.-
The wear experiment was conducted on couples consisting of iron, nickel, Fe-36% Ni and 3% silicon steel pins sliding against a tool steel disc. It has been found that the wear rate in air at room temperature lis independent to me hardness. The experimental observations are well related to the oxidation characteristics. However, the rate of oxidative wear is much higher than that for static oxidation due to the difference in the activation energy for oxidative wear. The lower energy for oxidational wear indicates that the rubbing surfaces are mechanically activated and high diffusivity path for diffusion of matrix elements and oxygen are produced during the sliding motion. The higher wear rate for cold-worked samples than for the annealed ones are associated with the higher oxidation rate for the cold-worked specimen.
Investigation of the Incorporation Efficiency of $\beta$-Carotene into Liposomes
Rhim, Chae-Hwan,Lee, Kyong-Eun,Yuk, Hyun-Gyun,Lee, Sang-Chun,Lee, Seung-Cheol The Korean Society of Food Science and Nutrition 2000 Preventive Nutrition and Food Science Vol.5 No.3
Chemical and photochemical precesses during food storage an preparation rapidly degrade $\beta$-carotene, the most active form of carotenoids. We investigated the possibility of liposomes as tool to preserve $\beta$-carotene. Liposomes with $\beta$-carotene were prepared as multilamellar vesicles by using soybean phosphatidylcholine, in terms of the ratio of $\beta$-carotene to phospholipid and pH. Incorporated efficiency was 99.7% at 1:0.05 of phospholipid : $\beta$-carotene and at pH 9.0. As the concentration of $\beta$-carotene increased, the incorporated efficiency increased progressively. pH did not affect the incorporation efficiency greatly.
Antiviral effect of Wild Oyster mushroom (Pleurorus ostereatus) against respiratory virus
Rhim Ryoo,Hyorim Lee,Mi-Jeong Park,Eunjin Kim,Ki Won Lee 한국식품영양과학회 2021 한국식품영양과학회 학술대회발표집 Vol.2021 No.10
Oyster mushroom (Pleurorus ostereatus) is popular as a healthy diet food due to their richness in essential amino acids and low calories. Also, the need for functional research on disease prevention using this mushroom has been increased. Thus, our study tried to evaluate the antiviral activity against viruses that cause human infection by using hot water extract of oyster mushroom. The material used in this study was the fruiting bodies of this mushroom which were collected from Ginko biloba in Yongmunsa, Kapyung in 2018. For the antiviral activity test, the aqueous extract of the mushroom was prepared by incubating 50g of the dried fruiting body powder in 500 ml of distilled water at 100°C for 2 hours. Antiviral activity was performed with the novel swine-origin influenza A (H1N1) virus by modified ASTM E1052-11 method using plaque assay. As a result of measuring the decrements in the virus for 2 hours, this extract showed 99.99% antiviral efficacy against influenza A (H1N1) virus. This result suggest that the boiled oyster mushroom extract has a high application value for the prevention of viral respiratory diseases as a personalized food through drinking material in daily life.
Verilog-A behavioral model for resonance-modulated silicon micro-ring modulator.
Rhim, Jinsoo,Ban, Yoojin,Yu, Byung-Min,Lee, Jeong-Min,Choi, Woo-Young Optical Society of America 2015 Optics express Vol.23 No.7
<P>We present an accurate behavior model for Si micro-ring modulators (MRM) based on Verilog-A, a standard simulation tool for electronic system design. Our model describes the electrical characteristics of the Si MRM using an equivalent circuit and the optical characteristics based on the couple-mode theory. The accuracy of our model is confirmed by comparing simulation results of our behavior model with the measurement results of a fabricated Si MRM. With this behavior model, co-simulation of Si MRM and electronic driving circuits in the standard electronic design environment can be easily performed.</P>
Rhim, E.M.,Ahn, S.J.,Kim, J.Y.,Chang, Y.R.,Kim, K.H.,Lee, H.W.,Jung, S.H.,Kim, E.C.,Park, S.H. Academic Press 2013 Cryobiology Vol.67 No.2
Cryopreservation is used to protect vital periodontal ligaments during the transplantation of teeth. We investigated which gene products implicated in root resorption are upregulated in human periodontal ligament cells by cryopreservation, and whether cryopreservation affects the expression of macrophage-colony stimulating factor (M-CSF) in human periodontal ligament cells. We used customized microarrays to compare gene expression in human periodontal ligament cells cultured from teeth immediately after extraction and from cryopreserved teeth. Based on the result of these assays, we examined M-CSF expression in periodontal ligament cells from the immediately extracted tooth and cryopreserved teeth by real-time PCR, enzyme-linked immunosorbent assay (ELISA), Western blot analysis, and immunofluorescence. We also investigated whether human bone marrow cells differentiate into tartrate-resistant acid phosphatase (TRAP) positive osteoclasts when stimulated with RANKL (Receptor Activator for Nuclear Factor κ B Ligand) together with any secreted M-CSF present in the supernatants of the periodontal ligament cells cultured from the various groups of teeth. M-CSF was twofold higher in the periodontal ligament cells from the rapid freezing teeth than in those from the immediately extracted group (p<0.05). Cryopreservation increased M-CSF expression in the periodontal ligament cells when analyzed by real time PCR, ELISA, Western blotting, and immunofluorescence (p<0.05). TRAP positive osteoclasts were formed in response to RANKL and the secreted M-CSF present in the supernatants of all the experimental groups except negative control. These results demonstrate that cryopreservation promotes the production of M-CSF, which plays an important role in root resorption by periodontal ligament cells.