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Sankar Ganesh, R.,Sharma, Sanjeev K.,Abinnas, N.,Durgadevi, E.,Raji, P.,Ponnusamy, S.,Muthamizhchelvan, C.,Hayakawa, Y.,Kim, Deuk Young Elsevier Sequoia S.A 2017 Materials chemistry and physics Vol.192 No.-
<P><B>Abstract</B></P> <P>Nanostructured bismuth titanate (Bi<SUB>4</SUB>Ti<SUB>3</SUB>O<SUB>12</SUB>) or BTO powders were synthesized by the combustion method. The crystalline phase of BTO nanopowders was evaluated from X-ray diffraction (XRD) and further confirmed by selected area electron diffraction (SAED) pattern. The SEM and TEM micrographic images clearly showed the nanosheets like morphology of BTO nanopowder. The EDS spectrum of BTO nanopowder showed the elemental peaks of O, Bi and Ti at 0.53 keV, 2.41 keV and 4.49 keV, respectively. FTIR band peaks were observed at 815 and 595 cm<SUP>−1</SUP> corresponding to the stretching vibrations of BiO and TiO. The red shift in optical absorption of BTO was observed and the bandgap decreased from 3.18 to 3.08 eV as the calcined temperature increased from 600 to 800 °C. The sandwich structure, called the nanogenerator, Graphene/BTO-PDMS/Graphene (G/BTO/G), was fabricated on graphene coated polymethyl methacrylate (PMMA) substrates, which produced a peak voltage (10 mV) by applying the pressure from human's finger. The switching mechanism of BTO nanosheets was observed to be dependent on the polarity and intrinsic dipole formation.</P> <P><B>Highlights</B></P> <P> <UL> <LI> Bi<SUB>4</SUB>Ti<SUB>3</SUB>O<SUB>12</SUB> (BTO) nanosheets synthesized from a simple combustion method. </LI> <LI> SEM & TEM images confirmed the nanosheets structure with a hexagonal shape. </LI> <LI> XRD and SAED pattern of BTO nanosheets confirmed the orthorhombic crystal structure. </LI> <LI> Flexible G/BTO/G nanogenerator fabricated by sol-gel method. </LI> <LI> Peak voltage was observed to be 10 mV by applying pressure from human's finger. </LI> </UL> </P> <P><B>Graphical abstract</B></P> <P>[DISPLAY OMISSION]</P>
Photocatalytic properties of Mn-doped NiO spherical nanoparticles synthesized from sol-gel method
Sankar, S.,Sharma, Sanjeev K.,An, Namhyun,Lee, Hwauk,Kim, Deuk Young,Im, Young Bin,Cho, Yung Duk,Ganesh, R. Sankar,Ponnusamy, S.,Raji, P.,Purohit, L.P. Elsevier 2016 OPTIK -STUTTGART- Vol.127 No.22
<P><B>Abstract</B></P> <P>Mn-doped NiO (NiO:Mn) nanopowders were synthesized from an inexpensive sol-gel method. The XRD peak profile analysis of NiO:Mn nanopowders confirmed the cubic structure. The spherical nanoparticles of NiO:Mn were evaluated from the SEM and TEM analysis and the grain size decreased as the Mn concentration increased. The average crystallite size decreased from 35.44nm to 30.5nm and the bandgap increased from 3.79eV to 3.95eV as the Mn concentration increased from 0wt.% to 4wt.%. The photocatalytic properties of NiO:Mn nanopowders were measured for the lowest and highest Mn dopant concentrations (Mn: 0 & 4wt.%) by using the methylene blue dye under UV illumination. The NiO:Mn (Mn: 4wt.%) nanoparticles showed the highest photocatalytic activity due to the highest activation sites. Therefore, it is revealed that the Mn: 4wt.% nanoparticles are observed to be more suitable for the photocatalytic activity of methylene blue dye degradation.</P>
Sankar Ganesh, R.,Sharma, S.K.,Sankar, S.,Divyapriya, B.,Durgadevi, E.,Raji, P.,Ponnusamy, S.,Muthamizhchelvan, C.,Hayakawa, Y.,Kim, D.Y. ELSEVIER 2017 Current Applied Physics Vol.17 No.3
<P>Nanocrystalline BiFeO3 (BFO) powder was synthesized by sol-gel method and subsequent annealed at 100-500 degrees C. The microstructural analysis of BFO nanopowder confirmed the perovskite like structure of spherical nanoparticles annealed at 500 degrees C. The Raman spectrum of BFO nanoparticles showed the rhombohedrally structure with the space group of R3c. The XPS spectrum of BFO nanopowder showed the peaks of Bi, Fe, and O at the binding energy of 158.8, 711.75 and 529.2 eV, respectively. The piezoelectric properties of BFO nanoparticles were evaluated by making the sandwiched structure of graphene/BiFeO3-PDMS/graphene. The fabricated piezoelectric device demonstrated an output voltage of 0.4 V by applying the normal pressure from human finger on the device. (C) 2016 Elsevier B.V. All rights reserved.</P>
T.Vigneswari,P. Raji 한양대학교 세라믹연구소 2016 Journal of Ceramic Processing Research Vol.17 No.9
Magnesium substituted nickel ferrite nanoparticles are prepared by using citrate precursor method. Synthesized nanoparticlesare analyzed by X-ray diffraction (XRD), Scanning electron microscope (SEM), Energy Dispersive X-ray (EDX) Analysis,Fourier transform infrared (FTIR) and Vibrating sample magnetometer (VSM). The crystalline size of nanoparticles isestimated to be 17-70 nm by using Debye Scherrer formula, Modified Scherrer formula and Williamson-Hall method. Twomain peaks near 570-590 cm−1 and 400-470 cm−1 confirm the spinel structure. Substitution of Mg2+ ion increases the saturationmagnetization value up to x = 0.4 after that decreases. Yafet- Kittel angle value increases with increasing Mg2+ concentration.
R. Sankar Ganesh,Sanjeev K. Sharma,S. Sankar,B. Divyapriya,E. Durgadevi,P. Raji,S. Ponnusamy,C. Muthamizhchelvan,Y. Hayakawa,김득영 한국물리학회 2017 Current Applied Physics Vol.17 No.3
Nanocrystalline BiFeO3 (BFO) powder was synthesized by sol-gel method and subsequent annealed at 100e500 C. The microstructural analysis of BFO nanopowder confirmed the perovskite like structure of spherical nanoparticles annealed at 500 C. The Raman spectrum of BFO nanoparticles showed the rhombohedrally structure with the space group of R3c. The XPS spectrum of BFO nanopowder showed the peaks of Bi, Fe, and O at the binding energy of 158.8, 711.75 and 529.2 eV, respectively. The piezoelectric properties of BFO nanoparticles were evaluated by making the sandwiched structure of graphene/ BiFeO3-PDMS/graphene. The fabricated piezoelectric device demonstrated an output voltage of 0.4 V by applying the normal pressure from human finger on the device.