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Freddy Boscán,María J. Barandiaran,Maria Paulis 한국공업화학회 2018 Journal of Industrial and Engineering Chemistry Vol.58 No.-
Miniemulsion preparation by low-energy phase inversion temperature (PIT) was performed for laurylmethacrylate (LMA) using polyethoxylated non-ionic emulsifiers. The minimum emulsifier content(4.5 wt%) and maximum amount of monomer (33 wt%) that led to stable miniemulsions was optimizedand the corresponding miniemulsions polymerized. Depending on the polymerization temperature, aconventional miniemulsion polymerization or a nanoemulsion polymerization (NEP) mechanism werefollowed. The possible explanation for the change of the reaction mechanism has been presented. Moreover, the robustness of the PIT technique for industrial applications was confirmed by polymerizinga LMA/isobornyl acrylate superhydrophobic monomer mixture.