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Anomalous Weak Ferromagnetism in Electron-doped Nd_(1−x)Sr_xMnO_3 (0.50 ≤ x ≤ 0.62) Thin Films
Pawan Kumar,Ravikant Prasad,Hari Krishna Singh,Rakesh Kumar Dwivedi,Avanish Kumar Srivastava,Mangala Prasad Singh 한국물리학회 2011 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.59 No.4
In the present work we demonstrate that an anomalous weak ferromagnetism occurs in the composition range 0.50 ≤ x ≤ 0.62 in nanostructured thin films of Nd_(1−x)Sr_xMnO_3 (NSMO). Nanocrystalline thin films of overdoped manganite Nd_(1−x)Sr_xMnO_3 (<I>x</I> ∼ 0.50, 0.55, 0.60 and 0.62) on single crystal LaAlO_3 (001) substrates are grown by nebulized chemical spray pyrolysis technique. These single phase films possess average crystallite size ∼15 nm and the width of the grain boundaries is ∼1 - 2 nm. In the composition range 0.50 ≤ x ≤ 0.62, the ground state of NSMO is A-type antiferromagnetic (AFM) metallic. However, in the present films a broad paramagnetic (PM) to ferromagnetic (FM) transition is observed in all the compositions at T_C ∼ 226 K for x = 0.50 and 235 K for rest of the samples. All the films show a well-defined M-H hysteresis loop at 5 K. The coercivity (H_C) of these films is much larger than those having composition range 0.35 < x < 0.45. For x = 0.50 (0.62) film H_C = -1210 (-1484) Oe and +1162 (+1476) Oe. The asymmetry in coercivity suggests the presence of weak exchange bias effect in these films. It is observed that the FM ground state in these films have smaller magnetic moment per Mn atom than the expected full moment using the rigid model, we term this as a weak ferromagnetic (WFM) state arising due to the destabilization of the AFM ordering. We propose a possible scenario based on the combined effect of spin reorganization and enhanced orbital disordering in nanosized manganites, to explain the observed anomalous weak ferromagnetism in the A-type AFM spin ordered regime.
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