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Yanru Yin,Changna Wen,Ning Ma,Baoyan Wang,Lianying Zhang,Hongliang Li,Peizhi Guo 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2019 NANO Vol.14 No.9
Palladium and palladium-silver bimetallic nanocrystals have been synthesized hydrothermally by using environmental-friendly sodium alginate as the stabilizer and reducing agent. The pure palladium nanoparticles were spherical-like possibly due to the principle of the lowest surface energy, however, the formation of bimetallic palladium-silver nanoparticles was much more complicated, which was thinner and more irregular nanostructures than pure palladium nanoparticles. Electrochemical measurements showed that the electrocatalytic activity toward ethanol oxidation was increased first with the increase of silver content in bimetallic nanoparticles, from pure palladium of around 1070 mA/mg, to PdAg-20 of 1160 mA/mg and to PdAg-10 of 1750 mA/mg, and declined greatly at a high content of silver, approximately 279 mA/mg. Electrochemical stability test showed that PdAg-10 and PdAg-5 were the best and worst among four palladium-based samples, respectively. Based on the experimental data, the formation mechanism of pure palladium and palladium-silver bimetallic nanoparticles and the structure-property relationship of these samples have been discussed.
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Chao Ma,Xing Duan,Xiaoqian Guo,Hua Qiao,Lianying Zhang,Xianbiao Mao,Peidong Wu 대한금속·재료학회 2023 METALS AND MATERIALS International Vol.29 No.2
The deformation mechanisms of a rolled high-purity α-titanium plate under monotonic loading along the rolling direction(RD), transverse direction (TD), and normal direction (ND) are investigated by the Elastic Visco-Plastic Self-Consistent(EVPSC) model, which incorporates a Twinning and De-Twinning (TDT) scheme to describe twinning behavior duringstraining. In the EVPSC-TDT model, plastic deformation is assumed to be accommodated by prismatic, basal and pyramidal⟨c + a⟩ slip modes as well as the 10̄12 extension and 11̄22 contraction twin modes. Numerical results based on theEVPSC-TDT model are in good agreement with the corresponding experimental data. The tension–compression asymmetry,anisotropic initial yielding and strain hardening behavior are interpreted in terms of the predicted relative activities of variousdeformation modes, twin volume fractions and texture evolutions. It is demonstrated that twinning plays an important rolein tension–compression asymmetry and plastic anisotropy, which is closely related to the loading direction with respect tocrystal orientations in the initial texture. In addition, it can be concluded that the TDT scheme permits better performancein describing twinning-associated deformation behavior for the rolled high-purity α-titanium plate than the PredominantTwin Reorientation (PTR) model even when detwinning is not involved.
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