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Elucidating synthesis of noble metal nanoparticles/graphene oxide in freescavenger γ-irradiation
Jie Shi,Wanwei Jiang,Liangsen Liu,Miaolei Jing,Fengyan Li,Zhiwei Xu,Xing-xiang Zhang 한국물리학회 2019 Current Applied Physics Vol.19 No.7
Three representative noble metal (Ag, Au and Pt) nanoparticles decorated graphene oxide (NMNPs/GO) composites were fabricated via γ-irradiation without scavenger. The NMNPs/GO composites exhibited the pure and well-dispersed particles structure, which directly illustrated that the GO could be acted as scavenger to benefit reduction and growth of NMNPs. Compared with irradiated GO (IGO), the GO substrate of composites had the lower relative content of hydroxyl groups, meanwhile, the relative contents of carbonyl groups (Pt > Au > Ag) were increased with increasing valence of noble metal. Such results illustrated that the abundant hydroxyl groups could convert the hydrated electrons, hydroxyl and hydrogen radicals to promote the growth of NMNPs on the surface of GO. In addition, the Raman signals of Ag NPs/GO composites were significantly enhanced (6.18 fold more than pristine GO, respectively), exhibiting obvious surface-enhanced Raman scattering activity. Therefore, this paper revealed that the GO could convert the hydrated electrons and radicals to synthetizing NMNPs/GO composites during γ-ray irradiation.
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Toughening of melamine–formaldehyde foams and advanced applications based on functional design
Bing Song,Xueli Zhu,Wei Wang,Liang Wang,Xiaoyuan Pei,Xiaoming Qian,Liangsen Liu,Zhiwei Xu 한국공업화학회 2023 Journal of Industrial and Engineering Chemistry Vol.119 No.-
Owing to the intrinsic flame-retardancy, thermal stability, sound absorption, and easy processing, melamine–formaldehyde foams(MFs) have drawn substantial attention. Typically, the high-porosity and compressibilityof flexible MFs render them suitable for the construction of 3D templates and in thefabrication of porous N-doped carbon materials. But the widespread applications of MFs still suffer highbrittleness and low strength, calling for modifying and toughening MFs with more facile and economicalmethods, and much potential in advanced applications by functional design deserves further exploration. This review comprehensively summarized and evaluated the recent progress of the toughening methodsof MFs. We will also look into the applications of commercial MFs, carbonized MFs and foam-based compositesin flame retardancy and thermal management, oil/water separation, photothermal conversion,electrical energy storage, and other fields, aiming to give a guide for the preparation, modification, andexploitation of MFs both in traditional and emerging areas.
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