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Dry reforming of methane over Ni/SBA-15 catalysts prepared by homogeneous precipitation method
Qiulin Zhang,Jing Wang,Ping Ning,Tengfei Zhang,Mingzhi Wang,Kaixian Long,Jianhong Huang 한국화학공학회 2017 Korean Journal of Chemical Engineering Vol.34 No.11
Ni/SBA-15 catalyst was prepared by homogeneous precipitation method (Ni-HP) and used for dry reforming of methane (DRM). The related characterization results indicated that the Ni particles were highly dispersed with a size range of 2-5 nm. Compared with Ni/SBA-15 catalyst prepared by impregnation (Ni-IM), the reduction temperature of Ni-HP obtained from H2-TPR was greatly improved, suggesting the stronger metal-support interaction. After reacting at 700 oC for 100 h, the CH4 conversion of DRM over Ni-HP catalyst slightly decreased from 74.5% to 73.8%. While, for the Ni-IM catalyst, the CH4 conversion dropped from 61.7% to 37.3%. Furthermore, the average particle size of Ni-HP was 3.7 nm and 4.7 nm before and after the long-time stability test, respectively, ascribed to the good antisintering property. Although a certain amount of coke was produced, mainly with disorder filamentous carbon of basegrowth, the Ni/SBA-15 prepared by homogeneous precipitation exhibited excellent catalytic activity and stability.
Kaixian Ba,Bin Yu,Xiangdong Kong,Hua-Long Zhao,Jin-Song Zhao,Qi-Xin Zhu,Chun-He Li 제어·로봇·시스템학회 2017 International Journal of Control, Automation, and Vol.15 No.4
The highly integrated valve-controlled cylinder (HIVC) is the joint driver in the hydraulic drive leggedrobot motion process, with the inner-loop-control-based outer loop dynamic compliance control method of the hydraulicsystem adopted. Yet the dynamic compliance of the HIVC position inner loop control has effects on theaccuracy of the outer loop dynamic compliance control. Therefore, the dynamic compliance parallel compositiontheory of the HIVC position inner loop control is presented and its dynamic compliance is analyzed in this paper,based on the HIVC position control nonlinear mathematical model. Moreover, the multiple parallel branch dynamiccompliance compound compensation control method is also designed and the dynamic compliance parallel compositionis rearranged. The experimental results indicate that adopting the compensation control method can decreasethe dynamic compliance of the HIVC position control system dramatically, which would provide the inner loopdynamic compliance compensation control method of the robot with high accuracy and high robustness.
Carbon dioxide reforming of methane over MgO promoted Ni/CNT catalyst
Dehua Zhang,Guangcheng Wei,Yiru Wang,Jing Wang,Ping Ning,Qiulin Zhang,Mingzhi Wang,Tengfei Zhang,Kaixian Long 한국화학공학회 2018 Korean Journal of Chemical Engineering Vol.35 No.10
Carbon dioxide reforming of methane to syngas was investigated over a series of MgO promoted Ni/CNT catalysts. MgO played a critical role in improving the catalytic performance of Ni/CNT. The results showed that the addition of MgO strengthened the interaction of Ni and interior surface of CNT. Highly dispersed nickel particles with small size (less than 4.5nm) were also observed in MgO modified CNT. Otherwise, the NiO nanoparticles were facilely reduced over the catalyst prepared with a narrow size of CNT, as shown in H2-TPR. The reaction tests demonstrated that the Ni-based catalyst with an addition of MgO and narrow size of CNT exhibited better catalytic activity. Furthermore, the lifetime of Ni-based catalyst was prolonged effectively after adding MgO, attributed to the stabilization and dispersion of Ni particles and the effective restraint on the gasification of CNT.