http://chineseinput.net/에서 pinyin(병음)방식으로 중국어를 변환할 수 있습니다.
변환된 중국어를 복사하여 사용하시면 됩니다.
Synthesis of Nickel Hierarchical Microstructures by a Simple Hydrothermal Route
Guo Bin Cheong,Gui Chen Wei,Cheong Jun Hao,Song Tian Li 대한금속재료학회 ( 구 대한금속학회 ) 2009 ELECTRONIC MATERIALS LETTERS Vol.5 No.3
Nickel hierarchical microstructures have been synthesized from the reduction of nickel hydrazine complexes by a simple hydrothermal method. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and superconducting quantum interference device (SQUID). The results indicated that the Ni hierarchical microstructures are face-centered cubic phase with a size of 2-3 μm for a single hierarchical microstructure while some thick petals with a length in the range of 0.5-1.5 μm extrude around the surface. The value of coercivity reached 121 Oe at room temperature, which is vastly superior to that of bulk nickel. Parallel experiments showed that the hydrothermal reaction time and the presence of surfactant cetyltrimethylamonium bromide (CTAB) played important roles in the formation of such hierarchical morphology.
Kim, Sung Won,Oh, Chang Whan,Williams, Ian S.,Rubatto, Daniela,Ryu, In-Chang,Rajesh, V.J.,Kim, Cheong-Bin,Guo, Jinghui,Zhai, Mingguo Elsevier 2006 Lithos Vol.92 No.3
<P><B>Abstract</B></P><P>Petrological analysis, zircon trace element analysis and SHRIMP zircon U–Pb dating of retrogressed eclogite and garnet granulite from Bibong, Hongseong area, SW Gyeonggi Massif, South Korea provide compelling evidence for Triassic (231.4±3.3 Ma) high-pressure (HP) eclogite facies (M1) metamorphisms at a peak pressure–temperature (<I>P</I>–<I>T</I>) of ca. 16.5–20.0kb and 775–850°C. This was followed by isothermal decompression (ITD), with a sharp decrease in pressure from 20 to 10kb and a slight temperature rise from eclogite facies (M1) to granulite facies (M2), followed by uplift and cooling. Granitic orthogneiss surrounding the Baekdong garnet granulite and the ophiolite-related ultramafic lenticular body near Bibong records evidence for a later Silurian (418±8Ma) intermediate high-pressure (IHP) granulite facies metamorphism and a prograde <I>P</I>–<I>T</I> path with peak <I>P</I>–<I>T</I> conditions of ca. 13.5kb and 800°C. K–Ar ages of biotite from garnet granulites, amphibolites, and granitic orthogneisses in and around the Bibong metabasite lenticular body are 208–219Ma, recording cooling to about 310°C after the Early Triassic metamorphic peak. Neoproterozoic zircon cores in the retrogressed eclogite and granitic orthogneiss provide evidence that the protoliths of these rocks were ∼800 and ∼900Ma old, respectively, similar to the ages of tectonic episodes in the Central Orogenic Belt of China. This, and the evidence for Triassic HP/UHP metamorphism in both China and Korea, is consistent with a regional tectonic link within Northeast Asia from the time of Rodinia amalgamation to Triassic continent–continent collision between the North and South China Blocks, and with an eastward extension of the Dabie–Sulu suture zone into the Hongseong area of South Korea.</P>