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Eder Uzziel Pulido Barragán,Carlos Fernando Castro Guerrero,Ana María Zamudio,Ana Beatriz Morales Cepeda,Thomas Heinze,Andreas Koschella 한국섬유공학회 2019 Fibers and polymers Vol.20 No.6
Cellulose nanocrystals (CNC) were obtained from Typha domingensis (an invasive macrophyte) collected fromlagoons and wetlands in Altamira, Mexico. Cellulose extraction was carried out by a treatment with aqueous NaOH in a batchreactor followed by NaClO-bleaching and subsequent hydrolysis with sulfuric acid. The fibers were characterized by FourierTransform Infrared (FTIR) spectroscopy, X-ray diffraction (XRD), thermogravimetric analysis (TGA), scanning electronmicroscopy (SEM), and atomic force microscopy (AFM). The crystallinity of the cellulose fibers isolated from Typhadomingensis increased from 29 % (not treated fibers) to 73 % and the beginning of thermal degradation increased from 246 oCto 312 oC before and after the bleaching. The CNCs isolated from this plant show average values of 20 nm in diameter and 190 nmin length. Micrographs of the Typha domingensis fibers and the cellulose isolated therefrom as well as bleached celluloseindicate the removal of hemicellulose, lignin, and waxes from the fibers, which corroborates the XRD and FTIR results.