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Wu, Xiao-Yuan,Lu, Can-Zhong,Xia, Chang-Kun,Chen, Shu-Mei,Liu, Jiu-Hui,Chen, Li-Juan,Yang, Wen-Bin Korean Chemical Society 2006 Bulletin of the Korean Chemical Society Vol.27 No.8
Four isostructural amino-acid-based polyoxomolybdates, {$M(H_2O)_3(pro)Mo_4O_{13}$}$_2{\cdot}2H_2O$ (pro = proline, M = Co (1), Ni (2), Cu (3), Zn (4)), have been synthesized and structurally characterized by single crystal X-ray diffraction, elemental analysis, IR spectrum, TG analysis. The structures of 1-4 are layered networks built up from {$Mo_8O_{26}(pro)_2$}$^{4-}$ units and {$M(H_2O)_3O_3$} octahedra, the uncoordinated water molecules occupying the interlayer regions.