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( Chih Chun Hsieh ),( Tao Chih Chang ),( Dong Yih Lin ),( Ming Che Chen ),( Wei Te Wu ) 대한금속재료학회 ( 구 대한금속학회 ) 2007 METALS AND MATERIALS International Vol.13 No.5
The purpose of this study is to investigate the precipitation characteristics of σ phase in the fusion zone of stainless steel welds at various welding passes during a tungsten arc welding (GTAW) process. The morphology, quantity, and chemical composition of the δ-ferrite and σ phase were analyzed using optical microscopy (OM), a ferritscope (FS), a X-ray diffractometer (XRD), scanning electron microscopy (SEM), an electron probe micro-analyzer (EPMA), and a wavelength dispersive spectrometer (WDS), respectively. Massive δ-ferrite was observed in the fusion zone of the first pass welds during welding of dissimilar stainless steels. The σ phase precipitated at the inner δ-ferrite particles and decreased δ-ferrite content during the third pass welding. The σ and δ phases can be stabilized by Si element, which promoted the phase transformation of δ→σ + γ2 in the fusion zone of the third pass welds. It was found that the σ phase was a Fe-Cr-Si intermetallic compound found in the fusion zone of the third pass welds during multi-pass welding.
( Ming-Che Chen ),( Chih-Chun Hsieh ),( Weite Wu ) 대한금속재료학회 ( 구 대한금속학회 ) 2007 METALS AND MATERIALS International Vol.13 No.3
In this study, the Accumulative Roll Bonding (ARB) process was used with a snap-stack procedure to reduplicate an Al (1100)/Mg (AZ31) alloy. Samples underwent four rolling and stacking cycles four times, which produced a 24-layer structure. The ARB process creates a multilayer compound between Al/Mg layers with excellent bonding characteristics. The excellent bonding characteristics were due to atomic diffusion. Diffusion couples between Al and Mg were investigated to study the composition of the formation in the Al-Mg system. Layers of intermetallic compound (IMC) Al3Mg2 and Al12Mg17 were observed. The composition-depth curves of the diffusion zone were determined by electron microprobe analyses of the IMCs.
A 20–40 SECOND PROCESS FOR SYNTHESIS OF MULTI-WALLED CARBON NANOTUBES
YUAN-YAO LI,TING-CHI LIU,CHIH-CHE HSIEH,MASAKI SAGEHASHI,AKIYOSHI SAKODA 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2006 NANO Vol.1 No.2
We report on a 20–40 s process for growing aligned, uniformed, high purity multi-walled carbon nanotubes (MWNTs) using an alcohol lamp burner. With an appropriate catalyst precursor concentration, MWNTs can be grown on a Co-coated 304 stainless steel mesh under incomplete combustion conditions at 680–700°C. The process provides a rapid, easy, economic and safe method for the formation of carbon nanotubes. We suggest that the proposed method be considered as an educational kit for college or high school level experiments.