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Crystallization of Precursors to Forsterite and Chromium-Doped Forsterite
Park, Dong Gon Martin, M. Hogan E. Ober, Christopher K. Burlitch, James M. Cavin, O. Burl Porter, Wallace D. Hubbard, Camden R. 숙명여자대학교 자연과학연구소 1994 자연과학논문집 Vol.- No.5
The pyrolysis and crystallization of poly(mathacrylate) precursors and xerogels of forsterite and chromiumdoped forsterite were studied by in situ high-temperature, dynamic X-ray diffraction and thermal analysis. For both types of precursor, crystallization of forsterite occurred at lower temperature when doped with chromium. Also, exotherms above 700℃ occurred 50℃ lower when chromium was present. When residual carbon in the xerogels was more than ∼1%, an unidentified crystalline intermediate phase formed at ∼800℃. Conversion of the intermediate phase to forsterite was faster than amorphous material. Thus, full crystallinity was attained at a lower temperature when the xerogels had some residual carbon.
Crystallization of Precursors to Forsterite and Chromium-Doped Forsterite
Park, Dong Gon,Martin, M. Hogan E.,Ober, Christopher K.,Burlitch, James M.,Cavin, O. Burl,Porter, Wallace D.,Hubbard, Camden R. 숙명여자대학교 자연과학연구소 1994 자연과학논문집 Vol.- No.5
The pyrolysis and crystallization of poly(mathacrylate) precursors and xerogels of forsterite and chromiumdoped forsterite were studied by in situ high-temperature, dynamic X-ray diffraction and thermal analysis. For both types of precursor, crystallization of forsterite occurred at lower temperature when doped with chromium. Also, exotherms above 700℃ occurred 50℃ lower when chromium was present. When residual carbon in the xerogels was more than ∼1%, an unidentified crystalline intermediate phase formed at ∼800℃. Conversion of the intermediate phase to forsterite was faster than amorphous material. Thus, full crystallinity was attained at a lower temperature when the xerogels had some residual carbon.