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Nano-Attached Tungsten Particle Synthesis and Sintering Behaviors
Chulwoong Han,Hanshin Choi,Byoungmoon Kim 대한금속·재료학회 2013 METALS AND MATERIALS International Vol.19 No.5
The reduction of sintering temperatures in industrial processes is advantageous for both energy efficiency and material properties in powder metallurgy. Based on the well-known size effects of nano-particles on sintering processes, nano-particles were intentionally used as a homogeneous sintering activator for micro-particles in this study. Two kinds of tungsten bimodal feedstocks which consisted of nano-particles and microparticles were prepared and sintered by spark plasma sintering processed. Even at the low sintering temperature of 1,250 °C and the short sintering time of 300 sec, relatively high densities could be achieved. Depending on the content of the nano-particles in the charged feedstock, the sintered body exhibited different morphological features. Density, field emission scanning electron microscopy, transmission electron microscope was used for analysis.