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Thermal Evolution of BaO-CuO Flux as Sintering Aid for Proton Conducting Ceramic Fuel Cells
Biswas, Mridula,Hong, Jongsup,Kim, Hyoungchul,Son, Ji-Won,Lee, Jong-Ho,Kim, Byung-Kook,Lee, Hae-Weon,Yoon, Kyung Joong The Korean Ceramic Society 2016 한국세라믹학회지 Vol.53 No.5
The eutectic melt of BaO-CuO flux is known to be a potential sintering aid for $Ba(Zr,Y)O_3$ (BZY) electrolyte for proton-conducting ceramic fuel cells (PCFCs). A density of BZY higher than 97% of theoretical density can be achieved via sintering at $1300^{\circ}C$ for 2 h using a flux composed of 28 mol% BaO and 72 mol% CuO. In the present study, chemical and structural evolution of BaO-CuO flux throughout the sintering process was investigated. An intermediate holding step at $1100^{\circ}C$ leads to formation of various impurity compounds such as $BaCuO_{1.977}$, $Ba_{0.92}Cu_{1.06}O_{2.28}$ and $Cu_{16}O_{14.15}$, which exhibit significantly larger unit cell volumes than the matrix. The presence of such secondary compounds with large lattice mismatch can potentially lead to mechanical failure. On the other hand, direct heating to the final sintering temperature produced CuO and $Cu_2O$ as secondary phases, whose unit cell volumes are close to that of the matrix. Therefore, the final composition of the flux is strongly affected by the thermal history, and a proper sintering schedule should be used to obtain the desired properties of the final product.
RELATIVE ORDER AND RELATIVE TYPE BASED GROWTH PROPERTIES OF ITERATED P ADIC ENTIRE FUNCTIONS
Biswas, Tanmay The Kangwon-Kyungki Mathematical Society 2018 한국수학논문집 Vol.26 No.4
Let us suppose that ${\mathbb{K}}$ be a complete ultrametric algebraically closed field and $\mathcal{A}$ (${\mathbb{K}}$) be the ${\mathbb{K}}$-algebra of entire functions on K. The main aim of this paper is to study some newly developed results related to the growth rates of iterated p-adic entire functions on the basis of their relative orders, relative type and relative weak type.
Biswas Arunangshu,Pradhan Oishika,Thati Anand,Mukherjee Debdyuti,Sau Tapan K.,Roy Chowdhury Shubhajit 한국물리학회 2022 Current Applied Physics Vol.44 No.-
The article presents a combined theoretical and experimental study attempting to show how Pd nanoparticles (NPs) loading onto SnO2 substrate improves the acetone gas sensing performance. Pristine nanostructured SnO2 and Pd nanoparticles (Pd NPs) loaded SnO2 substrates have been prepared, characterized, and their acetone sensing performances have been measured. Experimental measurements have shown that Pd NP loading onto SnO2 suppresses the interfering effects of ethanol, water vapors, etc., and enhances the acetone sensor response, reversibility, response/recovery speeds, and signal-to-noise ratio. Various parameters like the adsorption energy, HOMO–LUMO energy gap, charge distribution, polarizability change, electrophilicity index, global hardness, etc., of several model systems, have been computed by using DFT. The computed parameters have been correlated with the conductivity, local reactivity, sensor response and selectivity, response/recovery times, etc., of the systems to understand the molecular-level effects of the Pd NP loading onto the SnO2 on the gas sensing process.
Effect of Enrobing and Adding Antioxidants on the Quality of Pork Patties
Biswas, A.K.,Keshri, R.C.,Kumar, Sunil Asian Australasian Association of Animal Productio 2003 Animal Bioscience Vol.16 No.9
The effect of applying edible coating and addition of antioxidants (butylated hydroxyanisole (BHA) plus butylated hydroxytoluene (BHT) in a 1:1 ratio) on pork patties were investigated prior to achieve desired physico-chemical, microbiological and sensory qualities. For this, five treatments were conducted as (i) control (neither coated nor antioxidants treated); (ii) coated without antioxidants treated; (iii) coated and antioxidants added in the batter mix only (100 ppm); (iv) coated and antioxidants added in meat mix (100 ppm) only; and (v) coated and antioxidants added both in the batter mix (50 ppm) and the meat mix (50 ppm). Addition of antioxidants both in the batter mix and the meat mix significantly (p<0.05) reduced the microbial loads and thiobarbituric acid (TBA) values. The TBA values significantly (p<0.05) increased up to day 14 and then progressively increased with the advancement of each interval of storage days up to 28 days. Total plate count significantly (p<0.05) increased with the increase in storage days.Coliform and Staphylococcus aureus were absent throughout the storage days in all samples. Staphylococcus aureus however, were present in the control group at day 14 and in enrobed (coated) patties (without antioxidants treated) at 28th day. Addition of antioxidants to batter mix and meat mix did not substantially enhance bacteriostatic activity. Application of coatings and antioxidants retarded the loss of firmness, flavor, changes in appearance and color, and also other sensory attributes. Control patties were better with respect to microbial quality and TBA values but had poorer sensory quality than coated patties.
Growth Hormone Gene Polymorphism and Its Effect on Birth Weight in Cattle and Buffalo
Biswas, T.K.,Bhattacharya, T.K.,Narayan, A.D.,Badola, S.,Kumar, Pushpendra,Sharma, Arjava Asian Australasian Association of Animal Productio 2003 Animal Bioscience Vol.16 No.4
The study was carried out in Sahiwal, Holstein Friesian, Jersey and crossbred cattle and Murrah, Bhadwari, Jaffarabadi, Nagpuri and Surti buffaloes maintained at different organized herds to work out the polymorphism at growth hormone locus and study its effect on birth weight. A 223 bp fragment of the gene was amplified and digested with Alu I restriction enzyme. Two alleles, L and V with three genotypes LL, LV and VV were observed in Jersey, Holstein and cross bred cattle. Sahiwal cattle and buffalo were monomorphic for this locus producing only one genotype LL and one allele L. The frequency of L allele was comparatively higher in Holstein and crossbred cattle while in Jersey breed, the frequency of this allele was intermediate. The effect of genotype on birth weight was significant and LV genotype had higher birth weight than other genotypes. Hence, LV genotype in Holstein Friesian favored higher birth weight.
Biswas, Tanmay The Honam Mathematical Society 2019 호남수학학술지 Vol.41 No.2
The main aim of this paper is to study some growth properties of composite entire functions on the basis of relative $(p,q)-{\varphi}$ type and relative $(p,q)-{\varphi}$ weak type where p and q are any two positive integers and ${\varphi}(r):[0,+{\infty}){\rightarrow}(0,+{\infty})$ be a non-decreasing unbounded function.
Thermal Stability of Phaseolus vulgaris Leucoagglutinin: a Differential Scanning Calorimetry Study
Biswas, Shyamasri,Kayastha, Arvind M. Korean Society for Biochemistry and Molecular Biol 2002 Journal of biochemistry and molecular biology Vol.35 No.5
Phaseolus vulgaris phytohemagglutinin L is a homotetrameric-leucoagglutinating seed lectin. Its three-dimensional structure shows similarity with other members of the legume lectin family. The tetrameric form of this lectin is pH dependent. Gel filtration results showed that the protein exists in its dimeric state at pH 2.5 and as a tetramer at pH 7.2. Contrary to earlier reports on legume lectins that possess canonical dimers, thermal denaturation studies show that the refolding of phytohemagglutinin L at neutral pH is irreversible. Differential scanning calorimetry (DSC) was used to study the denaturation of this lectin as a function of pH that ranged from 2.0 to 3.0. The lectin was found to be extremely thermostable with a transition temperature around $82^{\circ}C$ and above $100^{\circ}C$ at pH 2.5 and 7.2, respectively. The ratio of calorimetric to vant Hoff enthalpy could not be calculated because of its irreversible-folding behavior. However, from the DSC data, it was discovered that the protein remains in its compact-folded state, even at pH 2.3, with the onset of denaturation occurring at $60^{\circ}C$.
Biswas, P. V.,Kim, H. Y.,Ahn, J. H. Springer Science + Business Media 2017 JOURNAL OF MECHANICAL SCIENCE AND TECHNOLOGY Vol.31 No.4
<P>Manufacturing a high-pressure sensitive diaphragm type sensor is a complex task. Due to it's complex shape, several parts are designed individually. It involves welding of several parts. As welding involves several parameters it's difficult to control the welding geometry where it is being fused. So it is likely that the physical boundary condition of the welded region will be different from the theoretical boundary conditions. So the change in boundary condition will make the deflection of the diaphragm different. For a precision device, any effect of a change in boundary condition can affect the deflection of the diaphragm largely. Thus, any effect of imperfect welding in a high precision measuring device can hamper the sensitivity of the particular device. A welded diaphragm of steel for a pressure sensor using eddy current sensor to detect it's deflection due to pressure can lose it's effectivity, due to the unpredictable boundary conditions created after the welding. In this paper, we will be trying to find the cause of deviation between the theoretical and experimental results due to the effect of a change in boundary conditions at the welded region.</P>