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Phuc Nguyen Thien,Giang Nguyen Thi Huong,An Vu Nguyen Thien Truong,Nam Nguyen Thanh Hoai,Anh Ly Duc,Nguyen Huynh Cam,An Hoang,Phong Mai Thanh,Hieu Nguyen Huu 한국탄소학회 2023 Carbon Letters Vol.33 No.2
In this study, graphene oxide (GO) was synthesized by the improved Hummers’ method. The degree of oxidation from graphite (Gi) to GO was determined through interlayer spacing calculated from X–ray diffraction. Besides, the effect of KMnO4:Gi ratios (X1), H2SO4 volume (X2), oxidation temperature (X3), oxidation time of stage 1 (X4), and oxidation time of stage 2 (X5) was screened by the Plackett–Burman model. The simultaneous impact of three factors that influenced the degree of oxidation (X1, X2, and X3) was studied by the Box–Behnken experimental model of response surface methodology to achieve suitable conditions for the GO synthesis process. The characterization of GO product was investigated via the modern analytical methods: X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy, UV–Vis spectroscopy, field emission scanning electron microscopy, transmission electron microscopy, and atomic force microscopy. In addition, the study was also carried out on a pilot scale for orientation in industrial application with the yield of 14 g/batch.
Nguyen Luan Vu Truong,Hieu Giang Le,Thien Ngon Dang,Linh Le,Tat Linh Doan,Truong Thinh Nguyen,Moonyong Lee 제어로봇시스템학회 2013 제어로봇시스템학회 국제학술대회 논문집 Vol.2013 No.10
A unified method for the fractional-order proportional-integral controller based on IMC scheme (IMC-FOPI) is proposed. The analytical tuning rules are derived for achieving the performance improvement in terms of both disturbance rejection and set-point tracking. Many illustrative examples are considered to confirm the effectiveness of the proposed algorithm for both integer and fractional-order processes with time delays. In addition, the robust stability of fractional-order systems are also carried out in order to demonstrate that the proposed controller can hold well the robustness against perturbation uncertainty in the process models.