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관통형 속 빈 음극관 글로우 방전에서 다양한 음극관 디자인에 따른 구리방출선 세기 증가에 대한 연구
우정수,박현국,김용성,최규성,이상천,Woo, Jeong-Soo,Park, Hyun-Kook,Kim, Yong-Seong,Choi, Kyu-Seong,Lee, Sang-Chun 대한화학회 2004 대한화학회지 Vol.48 No.4
We have investigated the intensity of Cu 510.6 nm emission line in see-through hollow cathode glow discharge (st-HCGD) for the development of medical Cu vapor laser. In order to acquire the stable plasma in st-HCGD cell at high current, several factors such as current, the length and the inner diameter of cathode tube, the shape of the tube, and the range of the sputtering range were tested. An optimum condition in our st-HCGD cell was obtained at 600 V, 700 mA, 2.3 Torr of Ar gas (100 SCCM), and 40 mm of tube with 4-11-4 mm type cathode design. Also, it was indirectly observed that temperature in the cell could reach more than $1,000{\circ}C$ since Cu cathode was melt at the current more than 700 mA (melting point of Cu, $1084{\circ}C$). 의료용 구리증기 레이저 개발의 일환으로 관통형 속 빈 음극관 글로우 방전(seethrough Hollow Cathode Glow Discharge; st-HCGD)을 이용하여 Cu 510.6 nm 방출선의 세기 증가를 조사하였다. 높은 전류에서도 매우 안정한 플라스마가 생성될 수 있도록 여러 가지 요인들 - 작동 전압 및 전류, 음극관의 길이와 내경 및 내부 형태, 음극관의 sputtering range 등 - 에 따른 최적조건을 찾는 실험을 수행하였다. 그 결과, 최종적으로 디자인된 글로우 방전셀에서는 앞선 여러 가지 실험으로 최적화된 조건을 적용하였다. 이들 최적화된 조건으로는 방전셀 내부에 아르곤 가스를 100 SCCM(standard cubic centimeter)으로 일정하게 흘려주었을 때의 방전셀 압력은 2.3 Torr 이며, 방전 전압 및 전류는 600 V, 700 mA(420 W), 음극관의 형태는 4-11-4 mm, 음극관의 길이는 40 mm 등이다. 한편, 700 mA 이상의 고전류에서 녹은 구리 음극관을 관찰함으로써 음극 sputtering으로 인한 플라스마의 온도가 최소 $1,000{\circ}C$ 이상에 이르렀음을 확인할 수 있었다(구리의 녹는점, $1084{\circ}C$).
펄스전류 활성 소결에 의한 나노구조 Al2TiO5 화합물 제조 및 기계적 특성
강현수 ( Hyun Su Kang ),박현국 ( Hyun Kuk Park ),도정만 ( Jung Mann Doh ),윤진국 ( Jin Kook Yoon ),박방주 ( Bang Ju Park ),손인진 ( In Jin Shon ) 대한금속재료학회(구 대한금속학회) 2012 대한금속·재료학회지 Vol.50 No.11
Nano powders of Al2O3 and TiO2 compounds made by high energy ball milling were pulsed current activated sintered for studying their sintering behaviors and mechanical properties. The advantage of this process is that it allows very quick densification to near theoretical density and inhibition of grain growth. Nano-structured Al2TiO5 with small amount of Al2O3 and TiO2 was formed by sintering at 1300℃ for 5 minute, in which average grain size was about 96 nm. Hardness and fracture toughness of the nano-structured Al2TiO5 compound with a small amount of Al2O3 and TiO2 were 602 kg/mm2 and 2.6 MPa.m1/2, respectively.
HPLC용 Schiff Base 컬럼과 Glow Discharge 검출기의 개발에 관한 기초연구 I
강미라,김은수,신정숙,박현국,양정성,이상천,Kang, Mi-Ra,Kim, Eun-Soo,Shin, Jung-Sook,Park, Hyun-Kook,Yang, Jung-Sung,Lee, Sang C. 한국분석과학회 1995 분석과학 Vol.8 No.3
본 연구는 중금속 이온의 신속한 현장분석을 위하여 HPLC용 Schiff Base 컬럼과 Glow Discharge 검출기의 개발에 관한 연구결과를 정리한 것이다. 현재 사용한 컬럼의 소재로는 hydrazide Schiff base 리간드인 N, N'-oxalybis(salicylaldehydrazone) (OBSH), N, N'-malonylbis (salicylaldehydrazone) (MBSH), 그리고 N, N'-succinylbis(salicylaldehydrazone) (SBSH)들과 HPLC 컬럼용 고분자 수지인 poly(styrene divinylbenzene)를 혼합하여 그 특성을 관찰하고 앞으로의 HPLC용 컬럼으로서의 응용성을 살펴보았다. 다음으로 중금속 이온들의 효과적인 검출을 수행할 수 있는 검출기의 필요성에 따라 현재 본 연구실에서 새로 개발한 Hollow Cathode Glow Discharge-Atomic Emission Spectrometry(HCGD-AES)를 사용하여 금속이온의 검출을 수행하였다. 이때 리간드-수지 혼합 컬럼을 통하여 용리된 용리액 중의 구리, 루비듐, 납, 수은 등의 금속이온 검출을 시도하였고, 실험결과를 토대로 Schiff Base를 사용한 컬럼이 금속이온에 따라 선택성을 보여 주고 있음을 살필 수 있었다. 또한 금속이온의 검출을 위한 HPLC용 검출기의 개발을 글로우 방전을 이용하여 추진하고 있으며 이에 대한 기초실험 결과를 정리하였다. Schiff base ligand columns and glow discharge detector have been developed for the trace analysis of metal ions desolved in water. Various types of hydrazide Schiff base ligands have been used and, additionally, they were examined as a filling material of a HPLC column. The hydrazide Schiff base ligands used were N, N'-oxalybis(salicylaldehydrazone) (OBSH), N, N'-malonylbis(salicylaldehydrazone) (MBSH), and N, N'-succinylbis(salicylaldehydrazone) (SBSH). A mixture of Schiff base ligand and poly(styrene divinylbenzene) was examined and it showed a smooth flow of solution. The OBSH-polymer column demonstrated different effluent factors for different metal ions. Metal ions in eluates were detected by Hollow Cathode Glow Discharge-Atomic Emission Spectrometry(HCGD-AES). HCGD-AES showed good sensitivity and selectivity. This is only the preliminary results of new OBSH-polymer column and glow discharge detector.
Kim Ki wook(金基郁),Park Hyun kook(朴炫局) 대한한의학원전학회 2005 대한한의학원전학회지 Vol.18 No.2
By comparing 'Jing Mai(「經脈」)' and 'Jin Fu(「禁服」)', we are able to see that 'Jing Mai' has adopted many of its aspects from 'Jin Fu', which also enables us to conclude that 'Jing Mai' was made after 'Jin Fu', with the 'Ren Ying Cun Kou Mai Fa(人迎寸口脈法)' being considered important. 'Jing Mai' was made relatively late, during the last days of 'Xi Han(西漢)' or early days of 'Dong Han(東漢)'. Also 'Jing Mai' was written after 'Ying Qi(「營氣」)'. '12 Jing Mai' in 'Jing Mai' is based mainly on 'Yin Yang Shi Yi Mai Jiu Jing(『陰陽十一脈灸經』)' and has also referred to other meridian theories, modifying it again by theories of 'Jin Fu' and 'Ying Qi', forming the 'Jing Mai Lian Huan(經脈連環)' part. The major change in '12 Jing Mai' is that '6 Yang Jing(6陽經)' enters the abdominal and thoracic cavity, directly relating to 'Liu Fu(六腑)'. 'Ben Jing(本經)'s connection to 'Ben Zang' is referred to as 'Shu(屬)' and connection to 'Ben Zang(本臟)' is referred to as 'Lou(絡)', clarifying 'Biao Li Guan Xi(表裏關系)' inside and outslde and 'Zang Fu Xiang He(臟腑相合)' congruency. Looking at the pathological condition view of 'Jing Mai', the writer of 'Jing Mai Pian' has renewed it and has erased repeated symptoms of 'Suo Seng Bing(所生病)' that appears in 'Shi Dong Bing(是動病)'. If the wrong adoption of theories of previous generations are corrected and parts which do not comply with the text's original meaning and parts that posterities added are deleted, the ancient acupuncture theory preserved in this book is still a precious treasure.