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기포제(起泡劑)가 모르더의 제성질(諸性質)에 미치는 영향(影響)에 관한 실험적(實驗的) 연구(硏究)
성찬용 ( Sung Chan Yong ),황은 ( Hwang Eun ) 한국농공학회 1985 韓國農工學會誌 : 전원과 자원 Vol.27 No.1
This study was performed to obtain the basic data which can be applied to the use of foaming mortars. The data was based on the properties of foaming mortars depending upon various mixing ratios and addings to compare those of cement mortar. The foaming agents which was used at this experiment were pre-foamed type and mix-foaming type which is being used as mortar structures. The foaming mortar, mixing ratios of cement to fine aggregate were 1:1, 1: 2, 1 : 3 and 1 : 4. The addings of foaming agents were 0.0%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5% and 3.0% of cement weight. The results obtained were summarized as follows; 1. At the mixing ratio of 1 : 1, the lowest water-cement ratios were showed by foaming mortars, respectively. But it gradually was increased in poorer mixing ratio and decreased in more addition of foaming agent. The water-cement ratios were decreased up to 1. 8~22. 0% by G, 2. 2~24. 1 % by U and 0. 7~53. 1% by J foaming mortar than cement mortar. 2. At the mixing ratio of 1 : 1, the highest bulk densities were showed by foaming mortars, respectively. But, it gradually was decreased in poorer mixing ratio and more addition of foaming agent. The bulk densities were decreased up to 1. 4~20. 7% by G, 2. 3~23. 7% by U and 26. 5~56. 5% by J foaming mortar than cement mortar. Therefore, foaming mortar could be utilized to the constructions which need low strengths. 3. At the mixing ratio of 1:1, the lowest absorption rates were showed by foaming mortars, respectively. But, it gradually was increased in poorer mixing ratio and more addition of foaming agent. Specially, according to the absorption rate when immersed in 72 hours, the absorption rates were showed up to 1. 01~1. 24 times by G, 1. 03~1. 58 times by U and 1. 10~5. 91 times by J foaming mortar than cement mortar. It was significantly higher at the early stage of immersed time than cement mortar. 4. At the mixing ratio of 1:1, the lowest air contents were showed by foaming mortars, respectively. But, it gradually was increased in poorer mixing ratio and more addition of foaming agent. Air contents were contented up to 4. 0~17. 2 times by G, 5. 2~23. 2 times by U and 23. 8~74. 5 times by J foaming mortar than cement mortar. 5. At the mixing ratio of 1 : 1, the lowest decreasing rates of strengths were showed by foaming mortars, respectively. But, it gradually was increased in poorer mixing ratio and more addition of foaming agent. Specially, the strengths of 28 days were decreased 0. 4~2. 2% than those of 7 days by foaming mortar, respectively. Also, the correlations between compressive and tensile strength, compressive and ending strength, tensile and bending strength were highly significant as a straight line shaped, respectively. 6. The correlations between absorption rate, air content, compressive strength and bulk density, absorption rate, compressive strength and air content were highly significant, respectively. The multiple regression equations of water-cement ratio, bulk density, absorption ate, air content, compressive strength, tensile strength and bending strength were computed depending on a function of mixing ratio and addition of foaming agent. It was highly significant, respectively. 7. At the mixing ratio of 1 : 1, the highest strengths were showed by cement mortar and foaming mortars, by chemical reagents. But, it gradually was decreased in poorer mixing ratio. The decreasing rates of strengths were in order of H<sub>2</sub>SO<sub>4</sub>, HNO<sub>3</sub> and HCI, J, U, G foaming mortar and cement mortar. Specially, at the each mixing ratio, each chemical reagent and 3.0% of foaming agent, J foaming mortar was collapsed obviously. Therefore, for the structures requiring acid resistence, adding of foaming agent should be lower than 3.0%.
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기포제가 모르터의 제성질에 미치는 영향에 관한 실험적 연구
성찬용,황은,Sung, Chan-Yong,Hwang, Eun 한국농공학회 1985 한국농공학회논문집 Vol.27 No.1
This study was performed to obtain the basic data which can be applied to the use of foaming mortars. The data was based on the properties of foaming mortars depending upon various mixing ratios and addings to compare those of cement mortar. The foaming agents which was used at this experiment were pre-foamed type and mix-foaming type which is being used as mortar structures. The foaming mortar, mixing ratios of cement to fine aggregate were 1:1, 1: 2, 1 : 3 and 1 : 4. The addings of foaming agents were 0.0%, 0.5%, 1.0%, 1.5%, 2.0%, 2.5% and 3.0% of cement weight. The results obtained were summarized as follows; 1. At the mixing ratio of 1 : 1, the lowest water-cement ratios were showed by foaming mortars, respectively. But it gradually was increased in poorer mixing ratio and decreased in more addition of foaming agent. The water-cement ratios were decreased up to 1. 8~22. 0% by G, 2. 2~24. 1 % by U and 0. 7~53. 1% by J foaming mortar than cement mortar. 2, At the mixing ratio of 1 : 1, the highest bulk densities were showed by foaming mortars, respectively. But, it gradually was decreased in poorer mixing ratio and more addition of foaming agent. The bulk densities were decreased up to 1. 4~20. 7% by G, 2. 3~23. 7% by U and 26. 5~56. 5% by J foaming mortar than cement mortar. Therefore, foaming mortar could be utilized to the constructions which need low strengths. 3. At the mixing ratio of 1:1, the lowest absorption rates were showed by foaming mortars, respectively. But, it gradually was increased in poorer mixing ratio and more addition of foaming agent. Specially, according to the absorption rate when immersed in 72 hours, the absorption rates were showed up to 1. 01~1. 24 times by G, 1. 03~1. 58 times by U and 1. 10~5. 91 times by J foaming mortar than cement mortar. It was significantly higher at the early stage of immersed time than cement mortar. 4. At the mixing ratio of 1:1, the lowest air contents were showed by foaming mortars, respectively. But, it gradually was increased in poorer mixing ratio and more addition of foaming agent. Air contents were contented up to 4. 0~17. 2 times by G, 5. 2~23. 2 times by U and 23. 8~74. 5 times by J foaming mortar than cement mortar. 5. At the mixing ratio of 1 : 1, the lowest decreasing rates of strengths were showed by foaming mortars, respectively. But, it gradually was increased in poorer mixing ratio and more addition of foaming agent. Specially, the strengths of 28 days were decreased 0. 4~2. 2% than those of 7 days by foaming mortar, respectively. Also, the correlations between compressive and tensile strength, compressive and ending strength, tensile and bending strength were highly significant as a straight line shaped, respectively. 6. The correlations between absorption rate, air content, compressive strength and bulk density, absorption rate, compressive strength and air content were highly significant, respectively. The multiple regression equations of water-cement ratio, bulk density, absorption ate, air content, compressive strength, tensile strength and bending strength were computed depending on a function of mixing ratio and addition of foaming agent. It was highly significant, respectively. 7. At the mixing ratio of 1 : 1, the highest strengths were showed by cement mortar and foaming mortars, by chemical reagents. But, it gradually was decreased in poorer mixing ratio. The decreasing rates of strengths were in order of H $_2$S0 $_4$, HNO$_3$ and HCI, J,U,G foaming mortar and cement mortar. Specially, at the each mixing ratio, each chemical reagent and 3.0% of foaming agent, J foaming mortar was collapsed obviously. Therefore, for the structures requiring acid resistence, adding of foaming agent should be lower than 3.0%.
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강영호,이종현,황성찬,심준보,김응호,Kang, Young-Ho,Lee, Jong-Hyeon,Hwang, Sung-Chan,Shim, Joon-Bo,Kim, Eung-Ho 한국방사성폐기물학회 2007 방사성폐기물학회지 Vol.5 No.1
흑연음극을 이용하여 LiCl-KCl공융염내에서 금속우라늄의 전해정련을 수행하였다. Uraniurn-Graphite Intercalation Compound(U-GIC)의 형성에 의하여 우라늄 전착물의 sell-scraping이 일어나며 전해정련에서 stripping과정을 생략함으로서 전해효율을 높일 수 있다. 우라늄 전착물내의 희토류 원소 오염은 무시할 만 하였으나 약 300ppm정도의 탄소가 오염되어 있는 것으로 관찰되었다. 탄소 오염은 이트륨을 이용한 정제공정 등을 거칠 경우 제거 가능하리라 사료된다. 회수된 우라늄 전착물의 조직 특성을 분석하였으며, 스틸 음극에 의해 회수된 전착물과 비교하였다. 이 결과는 초기 실험결과 이며 보다 심층적 연구를 통하여 사용 후 금속핵연료의 전해정련 개념을 개선시킬 수 있을 것으로 판단된다.
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불화물 / 염화물 용융염을 이용한 우라늄금속의 전해정련에 관한 연구
강영호(Young Ho Kang),황성찬(Sung Chan Hwang),심준보(Joon Bo Shim),유재형(Jae Hyung Yoo) 한국공업화학회 2002 공업화학 Vol.13 No.1
본 연구에서는 KCI-LiCl과 LiF-NaF-KF(FLINAK)용융염에서 금속우라늄과 회토류를 원료물질로 하여 전해정련을 수행하였다. 음극 전착물의 주성분은 우라늄이었으며 다른 회토류 금속에 대한 우라늄의 분리계수는 염화물 용융염의 차이는 없었다. 용융염과 전착물내의 회토류의 농도는 회토류의 분해전압인 1.9V 이상의 인가전압에서 급격히 증가하였으며, 전류효율은 1.0~1.9V내에서 인가전압에 반비례하였다. The electrorefining experiments with an anode composed of U, Y, Gd, Nd and Ce were carried out in the KCl-LiCl and LiF-NaF-KF(FLINAK) eutectic melt at 500℃ and 600℃, respectively. Uranium was the major component in the cathode deposits, and the separation factors of uranium with respect to the rare earths (REs) were nearly same in both electrolytes. REs concentrations in the molten salts and cathode deposits increased sharply at above 1.9 V, which was decomposition voltage of REs. The current efficiency was inversely proportional to the applied voltage in the range of 1.0 V to 1.9 V (vs STS304 and Ni).
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용융염 전해정련 계에서 초 우라늄 대용물질로서 cerium dysprosium의 적용
강영호,황성찬,심준보,유재형 한국공업화학회 2003 공업화학 Vol.14 No.3
회토류원소 중 cerium과 dysprosium은 악틴족 원소와 염화물 생성 자유에너지의 차이가 크지 않기 때문에 분리하기가 매우 어렵다. 즉, 용융염을 사용 하는 전해정련 공정에서는 이들 회토류 원소가 악틴족 원소와 함께 석출되는 특성을 나타낸다. 이러한 성질을 이용하여 본 연구는 용융염을 전해질로 이용하는 전해정련실험에 cerium과 dysprosium금속을 초 우라늄원소의 대용 물질로 사용하여 그들의 모사 특성을 고찰하었다. 실험 결과 용융염 중 낮은 염화우라늄농도에서는 이 두 회토류 원소가 초 우라늄과 유사한 전해 특성을 나타냈으나, 높은 염화우라늄 농도에서는 회토류 원소의 거동을 보여주었다. The rare earth elements, especiaily cerium and dysprosium are very difficult to be separated from actinide elements due to their narrow differences in the Gibbs free energy of formation of chloride. That is, they are codeposited with actinide elements in electrorefining process with molten salt. Using this characteristics, present study discusses the feasibility for use of cerium and dysprosium metals to simulate the electrorefining characteristics of the transuranium. The experimental results show that the electrolytic behaviors of these two rare earth elements are similar with the transuranium in low concentration range of uranium chloride in molten salt. However, in high concentration range of uranium chloride they behave as the rare earth elements.
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