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고로(高爐)슬래그로 부터 제조(製造)된 용융(溶融)클링커의 광물조성(鑛物組成)과 색도특성(色度特性)
추용식,서성관,임두혁,송훈,이종규,이승호,Chu, Yong-Sik,Seo, Sung-Kwan,Im, Du-Hyuk,Song, Hun,Lee, Jong-Kyu,Lee, Seung-Ho 한국자원리싸이클링학회 2011 資源 리싸이클링 Vol.20 No.6
용융클링커 제조용 혼합원료 중의 하나로 고로슬래그를 사용하였다. 고로슬래그를 사용한 혼합원료는 용융클링커 제조를 위해 1620에서 용융하였다. 냉각된 클링커는 XRD 패턴으로 클링커 광물의 생성여부를, 색도분석기로 색도를 분석하였다. 용융클링커는 XRD 분석을 통해 OPC 광물과 동등의 클링커 광물을 포함하고 있다는 것을 확인할 수 있었다. 용융시멘트는 OPC보다 백색도가 높아, 색상이 OPC보다 옅게 관찰되었다. 용융시멘트의 LSF 및 SM이 높아짐에 따라 백색도는 낮아졌다. 또한 슬래그를 용융시켜 제조한 시멘트 클링커는 고로 슬래그시멘트보다 백색도가 높았다. Raw mix of molten clinker was fabricated using blast furnace slag as starting material. Raw mix was melted at 1620 for molten clinker fabrication. Color and mineral composition of molten clinker was investigated by XRD and colorimeter. It was found that the molten clinker contains alite and belite equivalent to OPC clinker mineral and shows higher whiteness value than that of OPC. Whiteness of the molten clinker decreased with LSF and SM. Also the whiteness value of the slag cement using molten clinker was higher than that of common slag cement.
유리연마슬러지를 사용한 다공성 소재의 미세구조 및 물리적 특성에 관한 연구
추용식,권춘우,이종규,심광보,Chu, Yong-Sik,Kwon, Choon-Woo,Lee, Jong-Kyu,Shim, Kwang-Bo 한국세라믹학회 2006 한국세라믹학회지 Vol.43 No.5
A porous material with a surface layer was fabricated from glass abrasive sludge and expanding agents. The glass abrasive sludges were mixed with expanding agents and compacted into precursors. These precursors were sintered in the range of $700-900^{\circ}C$ for 20 min. The sintered porous materials had a surface layer with smaller pores and inner parts with larger pores. The surface layer and closed pores controlled water absorption. As the expanding agent fraction and the sintering temperature increased, the porosity and pore size increased. The porous materials with $Fe_2O_3$ and graphite as the expanding agents had a low absorption ratio of about 3% or lower while the porous material with $CaCO_3$ as the expanding agent had a higher absorption ratio and more open pores.
유리연마슬러지를 사용한 경량골재 제조 및 골재의 내부기공이 물성에 미치는 영향에 관한 연구
추용식,이종규,심광보,Chu, Yong-Sik,Lee, Jong-Kyu,Shim, Kwang-Bo 한국세라믹학회 2005 한국세라믹학회지 Vol.42 No.1
유리연마슬러지와 graphite를 발포제로 사용하여 경량골재를 제조하였으며, 경량골재 내부기공과 물성과의 상관성을 도출하였다. 이때 graphite 함량을 각각 달리하여 성구를 제조하였으며, $700^{circ}C$ 및 $800^{circ}C$에서 20분 동안 소성하였다. 소성 전후 골제의 부피 변화를 검토한 결과, 발포제의 첨가량보다는 소성 온도가 즘 더 큰 영향을 미침을 확인하였다 기공의 크기 및 면적은 발포제 첨가량과 소성 온도 상승에 따라 증가하는 특징을 나타내었으나, 발포제 첨가량 $1\%$ 이상에서는 큰 폭의 증가를 동반하지 않았다. 흡수율/열전도율과 기공과의 상관성은 매우 높아, 각각의 상관관계계수는 $0.8\pm$ 이상을 나타내었다. Lightweight aggregate was made using glass abrasive sludge and graphite in this study. This study tried to draw the correlation between lightweight aggregate's properties and internal pore. The precursor was made by added different graphite contents and was burned for 20 min. at $700^{circ}C$ and $800^{circ}C$. The volume change of aggregate was checked at before and after homing, and confirmed that the homing temperature effected more than expanding agent on volume change. The size and area of pore in aggregate increased according to the amount of expanding agent and homing temperature but it didn't bring about big effect above $1\%$ of expanding agent. The absorbtion ratio, thermal conductivity and porosity have a high correlation, so each coefficient of correlation showed above $0.8\pm$.
추용식,정의종,송훈,이종규,김영곤,강대구,Chu, Yong-Sik,Jung, Ui-Jong,Song, Hun,Lee, Jong-Kyu,Kim, Young-Gon,Kang, Dae-Gu 한국세라믹학회 2010 한국세라믹학회지 Vol.47 No.5
ALC was fabricated using cement, lime and quartzite by hydrothermal reaction. ALC has low strength and brittleness on account of inner pores. The studies for resolving these problems were driven by many researchers. Among these researches, the controls of quartzite fineness have been studied for unsuitable properties of ALC. This study experimented with variation of 90 ${\mu}m$ residue for obtain good physical properties. It was found that 90 ${\mu}m$ residue influenced on physical properties of ALC. The lower amount of 90 ${\mu}m$ residue, the higher compressive and bending strength. But the continuing decrease of 90 ${\mu}m$ residue did not cause the increase of strength. In order to application of these results in process, the states of process and hydrothermal products will be considered.
추용식,서성관,임두혁,송훈,이종규,이승호,Chu, Yong-Sik,Seo, Sung-Kwan,Im, Du-Hyuk,Song, Hun,Lee, Jong-Kyu,Lee, Seung-Ho 한국세라믹학회 2011 한국세라믹학회지 Vol.48 No.6
Raw mix of molten clinker was fabricated using blast furnace slag as starting material. Raw mix was melted at 1620$^{\circ}C$ for molten clinker fabrication. It was found that molten clinker contained alite and belite equivalent to OPC clinker mineral by optical microscope and SEM. The size of alite was 10~50 ${\mu}m$ and that of belite was 20~80 ${\mu}m$. This result thought to be attributed low $Al_2O_3$ content and cooling condition. Interstitial phase increased with blast furnace slag content and gehlenite was formed by the condition of LSF and SM. So raw mix with 27~41% blast furnace slag could be converted into cement clinker by appropriate choice of melting andcooling methods in this study.
광학현미경을 이용한 소성 조건별 시멘트 클링커 광물의 특성 변화
추용식,김인섭,이종규,Chu, Yong-Sik,Kim, In-Seob,Lee, Jong-Kyu 한국세라믹학회 2004 한국세라믹학회지 Vol.41 No.11
광학 현미경을 사용한 시멘트 클링커의 특성 분석은 시멘트의 품질뿐만 아니라 제조공정도 예측 평가할 수 있다. 그러므로 본 연구에서는 광학 현미경(반사)으로 소성 조건을 달리한 클링커의 특성을 분석하였다. 승온 및 냉각 속도가 느려짐에 따라 alite와 belite는 성장하였으며, 특히 냉각 속도는 belite의 성장에 큰 영향을 주었다. 또한 최대 소성 온도에서의 유지 시간이 20분 증가함에 따라 alite와 belite가 약 5fm정도 성장하는 것을 확인하였으며, 최대 소성 온도가 140$0^{\circ}C$인 경우, belite의 크기는 양호하나 alite는 제대로 성장하지 않은 10~15$\mu\textrm{m}$수준이었다. The characteristic analysis of cement clinker using light microscope can evaluate not only the quality of cement but also making process. Thus this study analyzed clinkers having different burning conditions by reflective light microscope. As heating and cooling rates is decreased, alite and belite minerals grew and especially cooling rate had an effect on the growth of belite. Futhermore as the retention time in max. temperature got longer by twenty minutes, alite and belite minerals grew more about 5 $\mu\textrm{m}$. In the case of temperature 1400$^{\circ}C$ in max, the size of belite was suitable but alite was not suitable with the size of 10~15 $\mu\textrm{m}$.
C<sub>12</sub>A<sub>7</sub>계 슬래그와 석유 코크스 연소재를 사용한 수축저감재 및 모르타르의 특성
추용식,박수현,서성관,박재완,Chu, Yong Sik,Park, Soo Hyun,Seo, Sung Kwan,Park, Jae Wan 한국세라믹학회 2013 한국세라믹학회지 Vol.50 No.5
In this study, petroleum cokes ash and $C_{12}A_7$-based slag were used for the shrinkage reduction and strength enhancement of mortar. The hydration properties of shrinkage reduction agents were analysed. The flow, change of length and compressive strength were experimented with mortar-added shrinkage reduction agents. As a result of this study, petroleum cokes ash : $C_{12}A_7$-based slag = 60~80% : 20~40% showed excellent results. In the case of mortar with 20% $C_{12}A_7$-based slag, the setting time and change of length were similar to Ref. mortar. The flow and compressive strength were superior to Ref. mortar. In the case of mortar with a 40% $C_{12}A_7$-based slag, the setting time was longer than Ref. mortar. The compressive strength of 3 days and 7 days were superior to Ref. mortar.
페로니켈 슬래그로부터 Mg 이온의 용출특성과 화합물 제조
추용식,임유리,박홍범,송훈,이종규,이승호,Chu, Yong-Sik,Lim, Yoo-Ree,Park, Hong-Bum,Song, Hun,Lee, Jong-Kyu,Lee, Seung-Ho 한국세라믹학회 2010 한국세라믹학회지 Vol.47 No.6
Ferro-Nickel slag is one of the by-products in Ferro-Nickel manufacturing process. The slag is composed of $SiO_2$, MgO, $Fe_2O_3$ and others. But the slag has been buried at landfill despite having valuable elements. This study tried to extract Mg ion and fabricate Mg compound from ferro-nickel slag using hydrochloric acid solution. Mg ion was extracted with Si, Fe and other ions in HCl solution. So reprocess was needed for gaining high purity Mg ion. It was thought that Si ion or $SiO_2$ precipitated in HCl solution and removed from solution in filtering process. Fe ion converted into $Fe(OH)_3$ after reacted with $NH_4OH$ and precipitated in HCl solution. After these process, the filtrate was composed of high purity Mg ion. $MgCl_2{\cdot}NH_4Cl{\cdot}6H_2O$ was obtained through drying of filtrate and this product was changed into MgO by burning process ($600^{\circ}C$-30 min). That is, 1st material or solution for manufacturing 2nd product was fabricated using acid dissolution method and other treatments.
중석 광미를 사용한 시멘트 모르타르의 입도 및 수열합성온도별 물리적 특성
추용식,서성관,최성범,김경만,홍석환,Chu, Yong Sik,Seo, Seong Gwan,Choi, Sung Bum,Kim, Gyoung man,Hong, Seok Hwan 한국자원리싸이클링학회 2019 資源 리싸이클링 Vol.28 No.6
본 연구에서는 국내에 적절한 환경처리 없이 방치되어 있는 중석광미를 활용하여, 중석 광미 입도별 시멘트 모르타르 제조 후 수열합성온도별 물리적 특성을 확인하였다. 시멘트 모르타르 혼합 시 물-시멘트비는 75 %로, 모래-시멘트비는 400 %로 고정하였으며, 광미는 모래(모래 중량 대비 0 ~ 50 % )를 치환하여 사용하였다. 저비소 및 고비소 광미의 입경은 9.3 ~ 53.0 ㎛로 제어하였고 수열합성온도는 승온 속도 2 ℃로 고정하여 60 ~ 180 ℃에서 6시간 동안 유지하였다. 수열합성 온도가 증가에 따라 압축강도는 상승하였으며, 60분 분쇄 저비소 및 고비소 광미를 30 % 혼합 시 압축강도는 각각 55.2 MPa 및 54.5 MPa로, 비교시편 보다 300 % 이상 향상되는 결과를 도출하였다.