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생약제제 중 이산화황 잔류실태 시중 유통 생약제제 중 이산화황의 잔류실태 조사
이춘영(Chun-Yeong Lee),이정숙(Jeong-Sook Lee),이현경(Hyun-Kyung Lee),박원희(Won-Hee Park),김정곤(Jeong-Gon Kim),정애희(Ae-Hee Chung) 대한약학회 2012 약학회지 Vol.56 No.1
This study was carried out to investigate the content of sulfur dioxide residues in the medicine prepared from crue drugs. Total 29 pills that contains salvia miltiorrhiza root, anemarrhena rhizome, fritillaria bulb, glehnia root, asparagus tuber, lycium fruit, moutan root bark, cimicifuga rhizome, pinellia tuber, dipsaci radix, codonopsis pilosula root, liriope tuber, achyranthes root, prepared aconite, aurantii fructus immaturus, corydalis tuber, dioscorea rhizome were examined by the modified Monier_Willams method. Sulfur dioxide were detectd in all the tested samples, and were found over MRLs (30 mg/kg to medicinal herbs) in 8 samples (27.6%). Especilly, "i2" pills contains 132.46 mg/kg sulfur dioxide that is 4 times over than MRLs.
황영숙(Yuong-Sook Hwang),김양숙(Yang-Suk Kim),이성득(Sung-Deuk Lee),백수현(Soo-Hyun Baek),김경식(Gyung-Sig Kim),두옥주(Ok-Ju Tu),정보경(Bo-Kyung Jung),조진호(Jin-Ho Cho),정애희(Ae-Hee Chung),정의근(Eui-Geun Jung),장미라(Mi-Ra Jang),윤 환경독성보건학회 2003 환경독성보건학회지 Vol.18 No.4
This study was carried out to investigate the 106 kinds of pesticide residues in agricultural products (n =3,614) by GC, for the northern area of Seoul from March (1999) to December (2000). The detection rate of pesticide residues in samples was 5.0% (mean: 2.86±7.22 mg/kg, n=180). The order of the agricultural products in which pesticide residues were detected was korean lettuce> perilla leaf, pepper> chinese cabbage> leek> spinach. The percentage of the agricultural products in excess of MRL was 2.0% (n=73). The agricultural products in excess of MRL were korean lettuce(n=15), perilla leaf(n=13), leek (n=6), spinach(n=6), pepper (n=5). chwinamul (n=5), etc. The order of the pesticide residues which were detected in agricultural products was procymidone, endosulfan, chlorpyrifos, vinclozolin, chlorothalonil and diazinon. The average residual values of procymidone, endosulfan, chlorpyrifos, vinclozolin, chlorothalonil and diazinon were 4.07, 1.24, 1.27, 2.83, 17.71 and 1.48 respectively. The pesticide residues in excess of MRL were chlorpyrifos (n=19), endosulfan (n=12), procymidone (n=9), vinclozolin (n=6), etc, and the measured concentration ranges of chlorpyrifos, endosulfan, procymidone, vinclozolin, pyrazophos, diazinon and EPN were 0.03-6.72, 0.18-5.8, 2.0-60.8, 1.70-20.33, 0.26-1.21, 0.59-4.3 and 0.28-4.19 respectively.