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유동배소로상의 소결융착에 미치는 아연정광중의 Pb, Cu 의 영향에 관한 연구
박평주,백귀종 대한금속재료학회(대한금속학회) 1984 대한금속·재료학회지 Vol.22 No.11
A study on the effect of Pb and Cu in zinc ore is executed for a preventive measures of the fluidized bed agglomeration during the roasting of zinc concentrate. The more the contents of Pb and Cu in zinc concentrate increase, the more the amount of agglomeration increases. Especially, when the contents of Cu in zinc concentrate is over 2.5wt%, the roasting process is very hard. The more the roasting temperature increase, the more the amount cf agglomeration increases during the roasting of the concentrate (Pb 1.5%, Cu 0.7%), and the sorts of compound in agglomerating calcine get to be different. Namely, at 850-950℃, the agglomerating calcine contains ZnO, ZnO·Fe₂O₃,CuSO₄, 2PbO·PbSO₄4PbO·PbSO₄and 2PbO·SiO₂, etc.. At 800℃, 4PbO·PbSO₄is not contained, but at 750℃, ZnO, ZnO·Fe₂O₃, CuSO₄and PbSO₄are contained. When air blowing increases, the agglomeration decreases. In the effect for the change of particle size, when the size decreases, wt.% of bed agglomerating calcine decreases. In these experimental results for the preventive measures of the fluidized bed agglomeration, Pb and Cu in zinc concentrate must decrease less than 0.5%, 0.2% respectively, and air blowing must occasionally increase.
Hyeong Kyu Lim(임형규),Tran Thi Lan Anh(찬티난안),Sang Soo Yu(유상수),Kui-Jong Baek(백귀종),Young Eon Ihm(임영언),Dojin Kim(김도진),Hyojin Kim(김효진),Chang Soo Kim(김창수) 한국자기학회 2009 韓國磁氣學會誌 Vol.19 No.3
Magnetic phases of polycrystalline Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films were studied. The Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films were grown at 400 ℃ by using a molecular beam epitaxy. The Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films were p-type and electrical resistivities were 4.0 × 10<SUP>?2</SUP>~1.5 × 10<SUP>?4</SUP> ohm-㎝. Based on the analysis of magnetic characteristics and microstructures, it was concluded that the ferromagnetic phase formed on the Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB>/SiO₂/Si(100) thin films was Ge₃Mn? phase which has about 310 K of Curie temperature. Moreover, the Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin film which had Ge₃Mn? phase showed the negative magnetoresistance to be about 9% at 20 K when the magnetic field of 9 T was applied.
비정질 Ge<SUB>1 − x</SUB>Mn<SUB>x</SUB> 박막의 전기적, 자기적 특성에 미치는 열처리 효과
이병철(Byeong Cheol Lee),김동휘(Dong Hwi Kim),찬티난안(Tran Thi Lan Anh),임영언(Young Eon Ihm),김도진(Dojin Kim),김효진(Hyojin Kim),유상수(Sang Soo Yu),백귀종(Kui Jong Baek),김창수(Chang Soo Kim) 한국자기학회 2009 韓國磁氣學會誌 Vol.19 No.3
Amorphous Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> semiconductor thin films grown by low temperature vapor deposition were annealed, and their electrical and magnetic properties have been studied. The amorphous thin films were 1,000~5,000 A thick. Amorphous Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films were annealed at 300 ℃, 400 ℃, 500 ℃, 600 ℃ and 700 ℃ for 3 minutes in high vacuum chamber. X-ray diffraction analysis reveals that as-grown Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> semiconductor thin films are amorphous and are crystallized by annealing. Crystallization temperature of amorphous Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> semiconductor thin films varies with Mn concentration. Amorphous Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films have p-type carriers and the carrier type is not changed during annealing, but the electrical resistivity increases with annealing temperature. Magnetization characteristics show that the as-grown amorphous Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films are ferromagnetic and the Curie temperatures are around 130 K. Curie temperature and saturation magnetization of annealed Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films increase with annealing temperature. Magnetization behavior and X-ray analysis implies that formation of ferromagnetic Ge3Mn5 phase causes the change of magnetic and electrical properties of annealed Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> thin films.
비정질 Ge<SUB>1 − x</SUB>Mn<SUB>x</SUB> 박막의 자기수송특성에 미치는 열처리 효과
김동휘(Dong Hwi Kim),이병철(Byeong Cheol Lee),찬티난안(Tran Thi Lan Anh),임영언(Young Eon Ihm),김도진(Dojin Kim),김효진(Hyojin Kim),유상수(Sang Soo Yu),백귀종(Kui Jong Baek),김창수(Chang Soo Kim) 한국자기학회 2009 韓國磁氣學會誌 Vol.19 No.4
Amorphous Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> semiconductor thin films grown by low temperature vapor deposition were annealed at various temperatures from 400 to 700 ℃ for 3 minutes in high vaccum chamber. The electrical and magnetotransport properties of as-grown and annealed samples have been studied. X-ray diffraction patterns analysis revealed that the samples still maintain amorphous state after annealling at 500 ℃ for 3 minutes and they were crystallized when annealing temperature increase to 600 ℃. Temperature dependence of resistivity measurement implied that as-grown and annealed Ge<SUB>1 ? x</SUB>Mn<SUB>x</SUB> films have semiconductor characteristics, the increase of resistivity with annealling temperature was obseved. The 700 ℃-annealed sample exhibited negative magnetoresistance (MR) at low temperatures and the MR ratio was ~8.5% at 10 K. The asymmetry was present in all MR curves. The anomalous Hall Effect was also observed at 250 K.