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Fe-29%Ni-17%Co 저열팽창 합금의 피로 특성에 미치는 알파상의 영향
김민종,권진한,조규상,이기안,Kim, Min-Jong,Gwon, Jin-Han,Cho, Kyu-Sang,Lee, Kee-Ahn 한국재료학회 2014 한국재료학회지 Vol.24 No.9
The effect of alpha phase on the fatigue properties of Fe-29%Ni-17%Co low thermal expansion alloy was investigated. Two kinds of alloys (Base alloy and Alpha alloy) were prepared by controlling the minimal alloy composition. Microstructure observation, tensile, high-cycle fatigue, and low-cycle fatigue results were measured in this study. The Base alloy microstructure showed typical austenite ${\gamma}$ phase. Alpha alloy represented the dispersed phase in the austenite ${\gamma}$ matrix. As a result of tensile testing, Alpha alloy was found to have higher strengths (Y.S. & T.S.) and lower elongation compared to those of the Base alloy. High cycle fatigue results showed that Alpha alloy had a higher fatigue limit (360MPa) than that (330MPa) of the Base alloy. The Alpha alloy exhibited the superior high cycle fatigue property in all of the fatigue stress conditions. SEM fractography results showed that the alpha phase could act to effectively retard both fatigue crack initiation and crack propagation. In the case of low-cycle fatigue, the Base alloy had longer fatigue life in the high plastic strain amplitude region and the Alpha alloy showed better fatigue property only in the low plastic strain amplitude region. The fatigue deformation behavior of the Fe-29%Ni-17%Co alloy was also discussed as related with its microstructure.
Fe-29%Ni-17%Co 저열팽창 합금의 열팽창 특성에 미치는 냉간 가공 및 열처리의 영향
이기안 ( Kee Ahn Lee ),권진한 ( Jin Han Gwon ),박종혁 ( Jong Hyuk Park ) 대한금속재료학회(구 대한금속학회) 2015 대한금속·재료학회지 Vol.53 No.1
The changes to thermal expansion and mechanical properties by cold working were investigated in the Fe-29%Ni-17%Co (wt%) low thermal expansion alloy. The Fe-29%Ni-17%Co alloy was cold rolled gradually and prepared for plating with reduction ratios of 0%, 20%, 40%, 60%, and 80%. The effect of annealing on the property was also studied. Thermal expansion was measured from 25 ℃ to 600 ℃ using a vacuum differential dilatometer. We found that the thermal expansion coefficient (α30~400) slightly decreased (at a reduction ratio of 20%) and then remarkably increased (above reduction ratios of 40%) with increasing reduction ratios of cold rolling. The thermal expansion coefficient (α30~400) sharply decreased after heat treatment. Yield and tensile strengths continuously increased and elongation decreased by cold rolling. Microstructural observation and XRD analysis results showed that the α phase significantly increased as the reduction ratio increased. The slight decrease of the thermal expansion coefficient below a reduction ratio of 20% could be explained by the destruction of short-range ordering and decrease in grain size. The significant increase in the thermal expansion coefficient with cold rolling attributed to the appearance of the α phase. The correlation between the microstructural cause and invar effect of the low thermal expansion behavior is also discussed. (Received April 7, 2014)