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용매추출법에 의한 토양중의 미량 구리와 아연원소의 동시추출 및 정량에 관한 연구
정창웅,지석주,박종안 한국환경보건학회 1995 한국환경보건학회지 Vol.21 No.3
A rapid and selective co-extraction systems of copper and zinc-thiocyanate complex into various types of alkylamine for the simultaneous determination of two metal ions by atomic absorption spectrometry and ion chromatograph have been proposed. The quantitative extractions of Cu(II) and Zn(II) at 0.1 M-thiocyanate and 0.1 M-HCI were achieved with Aliquat 336-$CHCl_3$. The detection limits of Cu and Zn were 2 ppb and 0.9 ppb respectively.
티오황산착염생성과 고분자량알킬아민에 의한 구리(11)의 추출(제1보)
정창웅 순천향대학교 1992 논문집 Vol.15 No.1
Micro smount of copper(11)from 0.01M sodium thiosulfate solution can be quantitatively extracted with 1% Aliquat336-MIBK. The mechanism of the extraction of copper(11)as thiosulfate complex into Aliquat 336 was elucidated. The effect of organic diluents and diverse ions on the determination of copper by atomic absortion spectrometry were examined.
티오시안착염색성과 고분자량알킬아민에 의한 아연(11)의 추출(제2보)
정창웅 순천향대학교 1992 논문집 Vol.15 No.1
A rapid and selective extraction system for subsequent determination of micro-grams of Zn by atomic absorption spectrometry has been proposed. The quantitative extraction of Zn in thiocyanate and sulfuric acid media was achieved with Alamine 336-MIBK. The possible composition of the Zn-thiocyanate complex extracted into the organic phase was presumed as ?? from the extraction data. The detection limit of Zn was 0.9ppb. Analysis of Zn in agricultural water was performed by the proposed method.
Crown화합물과 분광광도법에 의한 미량 납의 분리 및 분석
이화구,한현택,정창웅 순천향대학교 기초과학연구소 1999 순천향자연과학연구 논문집 Vol.5 No.2
Ion-pair extraction of lead(Ⅱ) form varying concentration of HCI solution was studied employing crown ether in nitrobenzenc as the extractant. Lead(Ⅱ) complex was stripped into alkaline solution and Pb(DDTC)₂complex was replaced quantitatively with Cu(Ⅱ), this complex has maximum absorbance at 450㎚. Beer's law applied in the range of 1.5 ∼ 7.5 ㎍/mL of Pb(Ⅱ) and molar absorptivity is 8.3 × 10³L/mole·㎝.
용매추출에 의한 생체시료중 미량 카드뮴의 분리, 농축 및 정량에 관한 연구
정창웅 순천향대학교 기초과학연구소 1997 순천향자연과학연구 논문집 Vol.3 No.1
Trace amount of cadmium was quantitatively extracted with 1% Aliquat 336-MIBK from 0.2M potassium thiocyanate and 0.01M-HCl solution. Of various liquid anion exchangers were tested, Aliquat 336 was found to be most efficient. The detection limit for the determination of Cd was 0.7ppb and proposed method was applied to the determination of Cd in serum and standard copper concentrates.
용매추출과 원자흡수분광법에 의한 망간(Ⅱ)의 분리 및 분석에 관한 연구
정창웅,심유상 순천향대학교 기초과학연구소 2004 순천향자연과학연구 논문집 Vol.10 No.2
The extraction of Manganese form industrial wastewater and wastes are very important. A method is described for the separation and determination of Manganese(Ⅱ) with 0.4M-potassium thiocyanate and 3% Aliquat 336-CC14 by liquid-liquid extraction and flame atomic absorption spectrometry. Managanese(Ⅱ) have been stripped into HCI solution in the presence of foreign ions. Calibration curve showed that Beer's law obey in the range of 7 ppm. Determination of Manganese(Ⅱ) in seawater was performed by the proposed method.
이중추출과 분광광도법에 의한 미량 수은(Ⅱ)의 정량에 관한 연구
정창웅 순천향대학교 기초과학연구소 2004 순천향자연과학연구 논문집 Vol.10 No.2
A selective and highly sensitive spectrophotometric method has been developed for the determination of trace mercury(Ⅱ) with 0.3M-KSCN and 1% Aliquat 336-CHCI₃. Hg(Ⅱ)-thiocyanate complex was extracted into quaternary ammonium salt and stripped into 3M-HCIO₄ solution. Hg(Ⅱ)-Dithizone complex has maximum absorbance at 490㎚ and obeys Beer's law in the range of 0.2~0.8㎍/㎖ in aqueous solution. The molar absorptivity and Sandell's sensitivity are 1.6×10^(5) L/mole·㎝ and 1.25 ×10^(-3)㎍/㎠ respectively.
액체-액체추출과 원자흡수분광법에 의한 토양중 미량 코발트(Ⅱ)의 정량에 관한 연구
정창웅 순천향대학교 기초과학연구소 1997 순천향자연과학연구 논문집 Vol.3 No.1
A rapid and selective extraction system for the subsequent determination of trace Co(Ⅱ) by atomic absorption spectrometry has been proposed. The quantitative extraction of Co in thiocyanate and nitric acid media was achieved with Aliquat 336-MIBK. The detection limit of Co was 1.1 ppb and analysis of Co in NBS sample was performed by the proposed method.