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Li Yao,Xie Wang,Haitao Liu,Chaowen Lin,Liangyu Pang,Junwei Yang,Qingbin Zeng 한국공업화학회 2017 Journal of Industrial and Engineering Chemistry Vol.56 No.-
A simple and efficient method for the determination of Cd and Pb in water samples was developed byultrasound-assisted magnetic retrieval-linked ionic liquid dispersive liquid–liquid microextraction (UA-MR-IL-DLLME) preconcentration and graphite furnace atomic absorption spectrometry (GFAAS)detection. Ionic liquid (IL) [Hmim] [PF6] was used as the extractant, ammonium pyrrolidinedithiocarbamate (APDC) as the complexing agent and Fe3O4 nanoparticles as the sorbent, whileultrasound was applied to assist the dispersion of the extractant and accelerate the mass transfer process. The effect of different factors on the extraction efficiency including pH, IL volume, APDC amount,ultrasound extraction time, ultrasound desorption time and Fe3O4 amount was studied by a fractionalfactorial design to screen for the most important factors. Then a central composite design was used tooptimize the significant factors. Under the optimal conditions, the method has linear calibration curvesover the range of 0.3–20 ng/mL for Cd and 0.5–40 ng/mL for Pb, with correlation coefficients (R) of0.9990 and 0.9986 for Cd and Pb, respectively. The limits of detection were 0.1 ng/mL and 0.15 ng/mL withrelative standard deviations of 3.4% and 2.8% for Cd and Pb, respectively. Finally, the method wassuccessfully applied for the determination of Cd and Pb in the real water samples and satisfactoryrecoveries were achieved.
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Suppression of stray electrons in the negative ion accelerator of CRAFT NNBI test facility
Yang Yuwen,Wei Jianglong,Xie Junwei,Gu Yuming,Xie Yahong,Hu Chundong 한국원자력학회 2023 Nuclear Engineering and Technology Vol.55 No.3
Comprehensive Research Facility for Fusion Technology (CRAFT) is an integration of different demonstrating or testing facilities, which aim to develop the critical technology or composition system towards the fusion reactor. Due to the importance and challenge of the negative ion based neutral beam injection (NNBI), a NNBI test facility is included in the framework of CRAFT. The initial object of CRAFT NNBI test facility is to obtain a H0 beam power of 2 MW at the energy of 200e400 keV for the pulse duration of 100 s. Inside the negative ion accelerator of NNBI system, the interactions of the negative ions with the background gas and electrodes can generate abundant stray electrons. The stray electrons can be further accelerated and dumped on the electrodes or eject from the accelerator. The stray electrons, including the ejecting electrons, cause the unwanted particle and heat flux onto the electrodes and the inner components of beamline (especially the temperature sensitive cryopump). The suppression of the stray electrons from the CRAFT accelerator is carried out via a series of design and simulation works. The paper focuses the influence of different magnetic field configurations on the stray electrons and the character of the ejecting electrons.
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Macrokinetic Model for Gluconobacter oxydans in 2-keto-L-gulonic Acid Mixed Culture
Zhixiong Zhang,Xinjie Zhu,Ping Xie,Junwei Sun,Jingqi Yuan 한국생물공학회 2012 Biotechnology and Bioprocess Engineering Vol.17 No.5
A set of kinetic models have been developed for the production of 2-keto-L-gulonic acid from L-sorbose by a mixed culture of Gluconobacter oxydans and Bacillus megaterium. A metabolic pathway is proposed for Gluconobacter oxydans, and a macrokinetic model has been developed for Gluconobacter oxydans, where the balances of some key metabolites, ATP and NADH are taken into account. An unstructured model is proposed for concomitant bacterium Bacillus megaterium. In the macrokinetic model and unstructured model, the mechanism of interaction between Gluconobacter oxydans and Bacillus megaterium is investigated and modeled. The specific substrate uptake rate and the specific growth rate obtained from the macrokinetic model are then coupled into a bioreactor model such that the relationship between the substrate feeding rate and the main state variables, such as the medium volume, the biomass concentrations, the substrate,and the is set up. A closed loop regulator model is introduced to approximate the induction of enzyme pool during lag phase after inoculation. Experimental results demonstrate that the model is able to describe 2-keto-Lgulonic acid fermentation process with reasonable accuracy.
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