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Analysis of Wide-gap Semiconductors with Superconducting XAFS Apparatus
S. Shiki,N. Zen,M. Koike,M. Ukibe,Y. Kitajima,S. Nagamachi,M. Ohkubo,N. Matsubayashi 한국초전도학회 2012 Progress in superconductivity Vol.14 No.2
Fluorescent yield X-ray absorption fine structure (XAFS) spectroscopy is useful for analyzing local structure of specific elements in matrices. We developed an XAFS apparatus with a 100-pixel superconducting tunnel junction (STJ) detector array with a high sensitivity and a high resolution for light-element dopants in wide-gap semiconductors. An STJ detector has a pixel size of 100 μm square, and an asymmetric layer structure of Nb(300 nm)-Al(70 nm)/AlOx/Al(70 nm)-Nb(50 nm). The 100-pixel STJ array has an effective area of 1 mm2. The XAFS apparatus with the STJ array detector was installed in BL-11A of High Energy Accelerator Research Organization, Photon Factory (KEK PF). Fluorescent X-ray spectrum for boron nitride showed that the average energy resolution of the 100-pixels is 12 eV in full width half maximum for the N-K line, and The C-K and N-K lines are separated without peak tail overlap. We analyzed the N dopant atoms implanted into 4H-SiC substrates at a dose of 300 ppm in a 200 nm-thick surface layer. From a comparison between measured X-ray Absorption Near Edge Structure (XANES) spectra and ab initio FEFF calculations, it has been revealed that the N atoms substitute for the C site of the SiC lattice.
Analysis of Wide-gap Semiconductors with Superconducting XAFS Apparatus
Shiki, S.,Zen, N.,Matsubayashi, N.,Koike, M.,Ukibe, M.,Kitajima, Y.,Nagamachi, S.,Ohkubo, M. The Korean Superconductivity Society 2012 Progress in superconductivity Vol.14 No.2
Fluorescent yield X-ray absorption fine structure (XAFS) spectroscopy is useful for analyzing local structure of specific elements in matrices. We developed an XAFS apparatus with a 100-pixel superconducting tunnel junction (STJ) detector array with a high sensitivity and a high resolution for light-element dopants in wide-gap semiconductors. An STJ detector has a pixel size of $100{\mu}m$ square, and an asymmetric layer structure of Nb(300 nm)-Al(70 nm)/AlOx/Al(70 nm)-Nb(50 nm). The 100-pixel STJ array has an effective area of $1mm^2$. The XAFS apparatus with the STJ array detector was installed in BL-11A of High Energy Accelerator Research Organization, Photon Factory (KEK PF). Fluorescent X-ray spectrum for boron nitride showed that the average energy resolution of the 100-pixels is 12 eV in full width half maximum for the N-K line, and The C-K and N-K lines are separated without peak tail overlap. We analyzed the N dopant atoms implanted into 4H-SiC substrates at a dose of 300 ppm in a 200 nm-thick surface layer. From a comparison between measured X-ray Absorption Near Edge Structure (XANES) spectra and ab initio FEFF calculations, it has been revealed that the N atoms substitute for the C site of the SiC lattice.
COMPUTER SIMULATION OF MAGNETIC PROPERTIES OF SPRING MAGNETS
N. Kitajima,H. Inoue,Y. Kanai,H. Fukunaga 한국자기학회 1995 韓國磁氣學會誌 Vol.5 No.5
Magnetic properties of model exchange-spring magnets, which are composed of magnetically soft and hard grains, were calculated by means of computer simulation. The dependence of the magnetic properties on the strength of intergrain exchange interaction and the amount of soft grains was studied. The existence of soft grains enhanced the remanence remarkably, and the remanence over 0.8Ms was obtained in the model magnets containing 25% or more soft grains by volume. The calculated coercivity vs. the strength of the exchange interaction curves showed a peak at a critical strength of the exchange interaction, although the remanence increased monotonously with increase in the strength of the exchange interaction. Thus the maximum energy product also reached a peak around the same critical strength. The calculated maximum energy product exceeded 300kJ/㎥ when the magnet is assumed to be composed of Fe₃B and Nd₂Fe₁₄B.
Anthraquinones from Cell Suspension Culture of Morinda elliptica
Jasril, Jasril,Lajis, N.H.,Abdullah, M.A.,Ismail, N.H.,Ali, A.M.,Marziah, M.,Ariff, A.B.,Kitajima, M.,Takayama, H.,Aimi, N. The Korean Society of Pharmacognosy 2000 Natural Product Sciences Vol.6 No.1
The chemical investigation on the cell suspension culture of Morinda elliptica L. yielded eight anthraquinones, two of which, anthragallol-1,2-dimethyl ether (3) and purpurin-1-methyl ether (4), have not been isolated from the original plant. Other compounds isolated include nordamnacanthal (1), alizarin-1-methyl ether (2), rubiadin (5), soranjidiol (6), $lucidin-{\omega}-methyl$ ether (7), and morindone (8). The structures of anthraquinones were established based on spectral studies.