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A Preliminary Study of Patchouli Oil Extraction by Microwave Air-Hydrodistillation Method
( Heri Septya Kusuma ),( Ali Altway ),( Mahfud Mahfud ) 한국화학공학회 2017 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.55 No.4
Patchouli oil extraction in general is still using conventional methods that require a long time of extraction. It is therefore necessary to develop extraction methods to obtain patchouli oil with optimum yield and quality. One of the new methods, which has been successfully developed, is microwave hydrodistillation (MHD). In addition to optimizing the extraction process of patchouli oil, this study also used microwave air-hydrodistillation (MAHD). Based on the research results, extraction using MAHD method can produce higher yield of patchouli oil when compared using MHD method. Also, based on the results of the analysis by GC-MS, extraction using MAHD method can produce quality of patchouli oil that is almost the same when compared using MHD method. This is supported by the results of the analysis by GC-MS, which showed that the content of patchouli alcohol is the main component of patchouli oil, and is almost the same for patchouli oil extracted using MHD method (26.32%) and MAHD method (25.23%).
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Heri Septya Kusuma,Ali Altway,Mahfud Mahfud 한국공업화학회 2018 Journal of Industrial and Engineering Chemistry Vol.58 No.-
Solvent-free microwave extraction method was first employed to extract essential oil from dried patchouli (Pogostemon cablin Benth) leaves. The effects of solvent-free microwave extraction variables including microwave power, ratio between mass of raw material with volume of distiller (F/D), raw material size and extraction time on the yield of essential oil were investigated. Meanwhile, the effects of solvent-free microwave extraction method in the chemical components of essential oil were also evaluated. The optimized conditions was as follows: microwave power of 450 W, ratio between mass of raw material with volume of distiller (F/D) of 0.06 g/mL, raw material size of intact (4.66 ± 1.41 cm) and extraction time of 90 min. Moreover, the extraction time was sufficient for solvent-free microwave extraction method to obtain higher yield than that using microwave hydrodistillation method for 3 h, indicating a significant reduction of extraction time and an improvement of efficiency. The composition of the essential oil was then determined by GC–MS, and 16 components were identified. The composition of essential oil obtained using solvent-free microwave extraction method meets the quality standard ISO 3757: 2002 (E), and the major component is patchouli alcohol (53.68%). This study suggests that solvent-free microwave extraction method is a rapid and efficient alternative for the extraction of essential oil from dried patchouli (P. cablin Benth) leaves, with a great potential for industrial application.
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( Heri Septya Kusuma ),( Taufik Imam Rohadi ),( Edwin Fatah Daniswara ),( Ali Altway ),( Mahfud Mahfud ) 한국화학공학회 2017 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.55 No.4
In Indonesia, vetiver oil is one commodity that plays an important role in the country`s foreign exchange earnings. Currently, the extraction of essential oil from vetiver still uses conventional methods. Therefore, the aim of this study was to know and verify the kinetics and mechanism of microwave hydrodistillation of vetiver based on two models. In this study, microwave hydrodistillation was used to extract essential oils from vetiver. The extraction was carried out in nine extraction cycles of 20 min to 3 hours. The rate constant, the equilibrium extraction capacity, and the initial extraction rate were calculated using the two models. Kinetics of oil extraction from vetiver by microwave hydrodistillation proved that the extraction process was based on the second-order extraction model. The second-order model was satisfactorily applied, with high coefficients of correlation (R<sup>2</sup> = 0.9427), showing that it well described the process.
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