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The free radical copolymerization and formation tendency of a charge transfer complex between acrylonitrile and N-vinyl phthalimidine was conducted in dimethyl formamide using benzoyl peroxide as an initiator. Copolymer formed was found to be consist...
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N-Vinyl Phthalimidine과 Acrylonitrile의 電荷轉移錯物 形成에 대한 硏究 = (A) Study on the Formation of a Charge Transfer Complex Between Acrylonitrile and N-vinyl Phthalimidine
한글로보기https://www.riss.kr/link?id=T736825
- 저자
-
발행사항
광주 : 朝鮮大學校 大學院, 1979
- 학위논문사항
-
발행연도
1979
-
작성언어
한국어
- 주제어
-
KDC
578 판사항(4)
-
발행국(도시)
광주
-
형태사항
26p. : 삽도 ; 26cm
-
일반주기명
참고문헌: p. 25-26
-
소장기관
- 경북대학교 중앙도서관
- 연세대학교 미래학술정보원
- 원광대학교 중앙도서관
- 조선대학교 도서관
- 경북대학교 중앙도서관
-
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부가정보
다국어 초록 (Multilingual Abstract)
The free radical copolymerization and formation tendency of a charge transfer complex between acrylonitrile and N-vinyl phthalimidine was conducted in dimethyl formamide using benzoyl peroxide as an initiator.
Copolymer formed was found to be consisted of the two monomer units in 1:l mole ratio.
Moreover, copolymerizati on rate was the maximum when the feed composition was 1:l in mole ratio.
The experimental conditions were [AN]_(0)=O.5×10^(-2)mole/liter, [NVPH]_(0)=0.73mole/liter∼3.75mol/liter and λ=340 and 345 nm, it was found that the equilibrium constant of the charge transfer complex calculated by using the Benessi-Hildebrand technique was 0.197 liter/mole.
This fact is closely related to form a charge transfer complex these two monomers. Activation energy of the copolymerization was found to be 4.2Kcal/mole.
Thermal and solubility behaviers of the copolymer were also examined.
Copolymer formed was found to be consisted of the two monomer units in 1:l mole ratio.
Moreover, copolymerizati on rate was the maximum when the feed composition was 1:l in mole ratio.
The experimental conditions were [AN]_(0)=O.5×10^(-2)mole/liter, [NVPH]_(0)=0.73mole/liter∼3.75mol/liter and λ=340 and 345 nm, it was found that the equilibrium constant of the charge transfer complex calculated by using the Benessi-Hildebrand technique was 0.197 liter/mole.
This fact is closely related to form a charge transfer complex these two monomers. Activation energy of the copolymerization was found to be 4.2Kcal/mole.
Thermal and solubility behaviers of the copolymer were also examined.
The free radical copolymerization and formation tendency of a charge transfer complex between acrylonitrile and N-vinyl phthalimidine was conducted in dimethyl formamide using benzoyl peroxide as an initiator.
Copolymer formed was found to be consisted of the two monomer units in 1:l mole ratio.
Moreover, copolymerizati on rate was the maximum when the feed composition was 1:l in mole ratio.
The experimental conditions were [AN]_(0)=O.5×10^(-2)mole/liter, [NVPH]_(0)=0.73mole/liter∼3.75mol/liter and λ=340 and 345 nm, it was found that the equilibrium constant of the charge transfer complex calculated by using the Benessi-Hildebrand technique was 0.197 liter/mole.
This fact is closely related to form a charge transfer complex these two monomers. Activation energy of the copolymerization was found to be 4.2Kcal/mole.
Thermal and solubility behaviers of the copolymer were also examined.
목차 (Table of Contents)
- 목차
- Abstract
- Ⅰ. 서론 = 1
- Ⅱ. 이론 = 6
- Ⅲ. 실험 = 8
- 목차
- Abstract
- Ⅰ. 서론 = 1
- Ⅱ. 이론 = 6
- Ⅲ. 실험 = 8
- 1. 시약 및 기기 = 8
- 2 . N-vinyl phthalimidine의 합성 = 9
- 3 . 혼성중합 = 12
- 4 . 흡광도 측정 = 13
- 5. 혼성중합체의 열 안정성 조사 = 14
- Ⅳ. 결과 및 고찰 = 14
- 1. 온도에 따른 반응 속도의 변화 = 14
- 2 . 혼성중합의 활성화 에너지 = 16
- 3. 혼성 중합 메카니즘 = 17
- 4. 흡광도에 의한 전하전이 착물 형성의 가능성 = 18
- 5. 혼성 중합체의 성질 = 22
- Ⅴ. 결론 = 23
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