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Preparation and characterization of HTSC LuBa2Cu3O6+x single crystals
V.E.Fedorov,M.Yu.Kameneva,N.V.Podberezskaya,D.Yu.Naumov,N.F.Beizel,U-HyonPaeka,L.P.Kozeeva 한양대학교 세라믹연구소 2002 Journal of Ceramic Processing Research Vol.3 No.3
For the first time large HTSC (high temperature superconductive) crystals of LuBa2Cu3O6+x (up to 5´5´0.2 mm3) were obtained from the Lu2O3-BaO-CuO system by a flux growth method. The crystals obtained were characterized by differential thermal analysis (DTA), chemical and X-ray diffraction analyses. The temperature of incongruent melting of the phase was defined more exactly (950±5oC). The composition of crystals corresponds to the formula LuBa2Cu3O6+x. The crystal structure of the tetragonal form was determined and x=0 was found for this case.