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- 저자 : Joaquina Orea-Lara (검색결과 1 건)
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Preparation and characterization of TiN powder by reactive milling in air
Joaquina Orea-Lara,Heberto Balmori-Ramírez,F. J. de Anda-Salazar,H. Yee-Madeira 한양대학교 세라믹연구소 2012 Journal of Ceramic Processing Research Vol.13 No.1
TiN powder was obtained by the reactive milling of a titanium powder in an air atmosphere, utilizing an attrition mill. Characterization of the powders was carried out by means of chemical analysis, X-ray diffraction (XRD), and scanning electron microscopy (SEM). The reaction took place over a period of 96 hours in the attrition mill. The XRD results indicate that a cubic TiN-like phase crystalline structure was produced in the mill, with a lattice parameter of 4.38 Å. The morphology of the obtained powders was nodular, having particle sizes within the nanometric size range. TiN powder was obtained by the reactive milling of a titanium powder in an air atmosphere, utilizing an attrition mill. Characterization of the powders was carried out by means of chemical analysis, X-ray diffraction (XRD), and scanning electron microscopy (SEM). The reaction took place over a period of 96 hours in the attrition mill. The XRD results indicate that a cubic TiN-like phase crystalline structure was produced in the mill, with a lattice parameter of 4.38 Å. The morphology of the obtained powders was nodular, having particle sizes within the nanometric size range.
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