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Chang-Lun Liao,Kuan-Hong Lin,Shun-Tian Lin 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.6
The microstructures and dielectric properties of Ba0.88(Nd1.40Bi0.42La0.30)Ti4O12/ alkali-borosilicate glass composites were investigated in this study, with the volume percentage of the glass phase in the composite being either 50, 55, or 60 vol.%. Sintered density measurements indicated that the density increased with an increase in the sintering temperature for the composites with 50 and 55 vol.% glass additions, but, at a sintering temperature higher than 800 oC, the density decreased for the composite with a 60 vol.% glass addition. XRD patterns revealed that the peak of the highest intensity in the B(NBL)T crystal belongs to the (401) crystal plane, while that in the B(NBL)T/glass composites to the (320) crystal plane. Along with the change in crystalline preferred orientation, the lattice constants of the crystal also changed. SEM micrographs indicated that the B(NBL)T phase developed into columnar grains at sintering temperatures higher than 1260 oC. Moreover, when glass was added, the grain morphology changed, especially at sintering temperatures higher than 850 oC. When sintered at 950 oC for 2 hours, the composite with 55 vol.% glass yielded the highest dielectric constant (εr= 23.2), the lowest dielectric loss (tanδ = 4.1 × 10-3), and a high Q×f value (Q × f = 1,620 GHz, Q = 1/tanδ, f = 6.67 GHz). The microstructures and dielectric properties of Ba0.88(Nd1.40Bi0.42La0.30)Ti4O12/ alkali-borosilicate glass composites were investigated in this study, with the volume percentage of the glass phase in the composite being either 50, 55, or 60 vol.%. Sintered density measurements indicated that the density increased with an increase in the sintering temperature for the composites with 50 and 55 vol.% glass additions, but, at a sintering temperature higher than 800 oC, the density decreased for the composite with a 60 vol.% glass addition. XRD patterns revealed that the peak of the highest intensity in the B(NBL)T crystal belongs to the (401) crystal plane, while that in the B(NBL)T/glass composites to the (320) crystal plane. Along with the change in crystalline preferred orientation, the lattice constants of the crystal also changed. SEM micrographs indicated that the B(NBL)T phase developed into columnar grains at sintering temperatures higher than 1260 oC. Moreover, when glass was added, the grain morphology changed, especially at sintering temperatures higher than 850 oC. When sintered at 950 oC for 2 hours, the composite with 55 vol.% glass yielded the highest dielectric constant (εr= 23.2), the lowest dielectric loss (tanδ = 4.1 × 10-3), and a high Q×f value (Q × f = 1,620 GHz, Q = 1/tanδ, f = 6.67 GHz).
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