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한복섭,이준희 대한의용생체공학회 1990 의공학회지 Vol.11 No.2
In order to use for artificial dental tooth (dental crowens) , new glass-ceramics material has been studied. Its basic composition and the condition of heat treatment for crystalization, mechanical and chemical properties were investigated. Adding of the LAS system composition in the basic glass, time and temperature for crystalization were shortened. Fracture toughness (kic)of samples heat treated at 90$0^{\circ}C$ for 2 hours is 2.5-2.6MN/m3/2, the optimum condition of heat treatment for artificial tooth is A and B samples heating to 75$0^{\circ}C$ for 2 hours, raising to 90$0^{\circ}C$ and maintaining at 90$0^{\circ}C$ for 2 hours and C sample heating to 75$0^{\circ}C$ maintaining at 75$0^{\circ}C$ for 2 hours. In acid and'alkali solution, chemical durability is excellent.
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인공치용 바이오 세라믹스의 제조 및 특성(II) 기계적 특성과 색도 및 색차변화
고영호,한복섭,이준희 한국세라믹학회 1995 한국세라믹학회지 Vol.32 No.10
The tests of three point bending and vickers hardness have been carried out to investigate mechanical characteristics of bioceramics for artificial dental crowns. And color and color difference test has been performed to study chromaticity changes after sintering specimens composited with glass and leucite powders. In addition, thermal dilation test has been carried out to examine bonding relations between dental porcelain and metal frame (Ni-Cr alloy). The result of three point bending test showed a maximum strength of about 68 MPa. Thermal expansion coefficient changed from 8.3$\times$10-6/$^{\circ}C$ to 13.5$\times$10-6/$^{\circ}C$ with increasing leucite content (0~30wt.%) in glass matrix. Bonding between porcelain (25% leucite-75% glass) and Ni-Cr alloy was excellent.
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유기수,한복섭 대한의용생체공학회 1993 의공학회지 Vol.14 No.3
A study on the biocompatibility of two types of new glass-ceramics materials, metal disc and dental porcelain that were already made for dental artificial tooth in the previous study, have been attempted. The chemical behavior and the Victor's hardness change in she artificial saliva and Ringer's solution have been also investigated. From the experiment of Implantation of glass-ceramics Into dorsal subcutaneous tissue of Sprague-Dawley rats, glass-cerarmics did not show any particular system of rejection for histrocompatibility.
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고영호,한복섭,이준희 동아대학교 공과대학 부설 한국자원개발연구소 1993 硏究報告 Vol.17 No.2
It has been investigated the Sintering Characteristics and Microstructure after the Manufacture of Dental Ceramics for Artificial Dental Tooth(Dental Crowns) in Dentistry. The Manufacture of High Thermal Expansional Leucite Crystals has been made by not Conventional Melting Process, but Sol-Gel Process, and composited with Class Frit that has low melting point to get Transparent Sintering Materials. The Crystal Forming Temperature of Leucite manufactured by Sol-Gel Process has been observed after Heat Treatment at various Temperatures. In Addition, The Manufacture Process is simpler than Conventional Melting Process and could be able to manufacture at about 400℃ low Temperature. Glass Frit that has low melting point was fabricated with about 10~30㎛ homogeneous amorphous Powders by means of Ball Milling and was transparent When fired. The Sintering Temperature could be controlled in accordance with the Powder Mixture of Leucite and Glass Frit. The Volume Fraction of Leucite Crystals in Glass Matrix has been increased by the appropriate Heat Treatment of Dental Porcelain.
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인공치용 바이오 세라믹스의 제조 및 특성 (1) : 제조 및 소결특성 Fabrication and Sintering Characteristics
고영호,한복섭,이준희,최석규,최진원 대한금속재료학회(대한금속학회) 1994 대한금속·재료학회지 Vol.32 No.10
Bioceramics for artificial dental crowns in dentistry have been fabricated by sol-gel process and melting method, respectively. Sintering characteristics have been investigated after compositing powder mixtures relative to leucite content(0∼30wt.%) added to glass matrix. Highly pure leucite powders have been fabricated by sol-gel process and glass powders have been manufactured with 20∼30㎛ particle size by a melting method. Sintering temperatures could be controlled from 1020℃ to 1175℃ relative to the powder mixtures of leucite and glass powders. The relative sintered density was 80∼83% of theoretical density. Shrinkage was about 20∼25% after sintering.
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