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- 주제어 : Y2BaCuO5 size (검색결과 2 건)
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Park, S.D.,Kim, H.J.,Park, B.J.,Han, Y.H.,Jun, B.H.,Lee, J.S.,Kim, C.J. North-Holland 2011 Physica. C, Superconductivity Vol.471 No.21
The effect of calcium doping on the superconducting properties of top seeded melt growth (TSMG) processed Y<SUB>1.5</SUB>Ba<SUB>2-x</SUB>Ca<SUB>x</SUB>Cu<SUB>3</SUB>O<SUB>y</SUB> superconductors was studied in terms of calcium content (X<SUB>ca</SUB>). YBa<SUB>2-x</SUB>Ca<SUB>x</SUB>Cu<SUB>3</SUB>O<SUB>7-δ</SUB> (X<SUB>ca</SUB>=0, 0.005, 0.01, 0.02, 0.04, 0.1, 0.3) powders were synthesized by the powder calcination method. YBa<SUB>2-x</SUB>Ca<SUB>x</SUB>Cu<SUB>3</SUB>O<SUB>7-δ</SUB> powders were mixed with 0.25mole Y<SUB>2</SUB>O<SUB>3</SUB> powder and 1wt.% CeO<SUB>2</SUB> as Y<SUB>2</SUB>BaCuO<SUB>5</SUB> (Y211) refiner, and finally made into Y<SUB>1</SUB>.<SUB>5</SUB>Ba<SUB>2-x</SUB>Ca<SUB>x</SUB>Cu<SUB>3</SUB>O<SUB>y</SUB> (Y1.5)+1wt.% CeO<SUB>2</SUB> composition. The single Y123 growth on the top surface was observed up to X<SUB>ca</SUB>=0.1, while the multiple Y123 growth was observed at X<SUB>ca</SUB>≥0.1. The superconducting transition temperature (T<SUB>c</SUB>) and critical current density (J<SUB>c</SUB>) of TSMG processed Y1.5 samples were inversely proportional to X<SUB>ca</SUB>. The Y211 size increased with increasing X<SUB>ca</SUB> due to the enhancement of Y211 coarsening by calcium doping. No Y211 refining effect by CeO<SUB>2</SUB> was observed in the calcium doped samples. The T<SUB>c</SUB> and J<SUB>c</SUB> decrease by calcium doping are likely to be due to the calcium incorporation with the Y123 lattice and formation of coarse Y211 particles.
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Youn, J.S.,No, K.,Kim, Y.H.,Mahmood, A.,Jun, B.H.,Han, Y.H.,Sung, T.H.,Kim, C.J. North-Holland 2009 Physica. C, Superconductivity Vol.469 No.15
To understand the effect of BaCeO<SUB>3</SUB> on a Y<SUB>2</SUB>BaCuO<SUB>5</SUB> (Y211) distribution, Y<SUB>1.5</SUB>Ba<SUB>2</SUB>Cu<SUB>3</SUB>O<SUB>x</SUB> (Y1.5) superconductors with/without 1wt.% BaCeO<SUB>3</SUB> additions were prepared by a top-seeded melt-textured growth (TSMG) process. Two different BaCeO<SUB>3</SUB> powders (as-synthesized (coarse powder) and an attrition-milled (fine powder)) were used and the size effect was compared with that obtained from a Y1.5 sample with no addition. A refinement of the Y211 particles was achieved for both the as-synthesized and attrition-milled BaCeO<SUB>3</SUB> additions. The distribution of the Y211 particles was most uniform in the Y1.5 sample prepared with the attrition-milled BaCeO<SUB>3</SUB> powder due to the reduced size of the Y211-free regions by the fine size BaCeO<SUB>3</SUB> addition. The highest J<SUB>c</SUB> was achieved in the Y1.5 sample prepared with the attrition-milled BaCeO<SUB>3</SUB> powder. The J<SUB>c</SUB> result agreed well with the microstructure variations by the addition of BaCeO<SUB>3</SUB> powders.
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