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Rongfeng Zhu,Qihui Zhang,Bijun Fang,Jianning Ding,Xiangyong Zhao,Haosu Luo 한국물리학회 2016 Current Applied Physics Vol.16 No.12
In situ temperature dependent ferroelectric domains dynamic evolution of the (001)pc oriented 0.91Pb(Zn1/3Nb2/3)O3-0.09PbTiO3 (PZNT91/9) single crystals was observed by polarized light microscopy (PLM) and real time synchrotron-radiation (SR) X-ray white-beam topography. Intricate domain structures including monoclinic phase are distinguished by PLM at room temperature, and irreversible domain configuration dynamic evolution upon thermal cycling is observed by both methods. Such irreversible domain evolution combined with coexistence of multi-phases and polarization rotation may be related to the extraordinary piezoelectric performance in the ferroelectric single crystals with the morphotropic phase boundary (MPB) compositions.
Deng Tingyu,Fang Bijun,Zhu Rongfeng,Chen Jianwei,Luo Haosu 한국물리학회 2021 Current Applied Physics Vol.21 No.-
Due to the good dielectric, piezoelectric and ferroelectric properties, the pseudo-ternary ferroelectric single crystals Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3 (PIN-PMN-PT) have been widely concerned and studied. In this study we found that the dynamic hysteresis loop area <A> with electric field E0 and frequency f0 of the 0.16 Pb(In1/2Nb1/2)O3-0.62 Pb(Mg1/3Nb2/3)O3-0.22PbTiO3 (0.16PIN-0.62PMN-0.22 PT) single crystals satisfies the relational equation <A> ∝ E0β f0α . In the <A> ∝ E0β relationship, both linear stages are found correlated with the low electric field in the first stage E0<Ec and the high electric field in the third stage E0 > 3Ec. The hysteresis loop area <A> with frequency f0 relationship satisfies the equation <A> ∝ f0α with roughly linear trend and the hysteresis loop area <A> decreases with increasing frequency f0. Such electric field dependent dynamic hysteresis scaling can be observed by polarized light microscopy.