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Qun Wei,Lei Xu,Zhimeng Tang,Zhangbiao Xu,Cheng Xie,Lirong Guo,Wei Li 한국공업화학회 2023 Journal of Industrial and Engineering Chemistry Vol.122 No.-
Herein, a facile preparation method with characteristics of energy-saving, efficient and environmentallyfriendly is proposed. Firstly, GICs (Graphite Intercalation Compounds) were synthesized by microwaveassisted hydrothermal method using flake graphite (FG) as raw material, H2SO4, and K2S2O8 as oxidativeintercalations by microwave-assisted oxidation for 5 min, and then EG was prepared from obtained GICsby microwave irradiation for 40 s under the microwave power of 800 W, and the effect of different processconditions on EG expansion volume (EV) was studied. The results show that EG with a good expansioncan be rapidly prepared by microwave irradiation, and the EV value can reach 455 mL /g under theoptimal conditions. In particular, the prepared EG has a high graphitization degree with less structuraldamage, exihibiting good industrial application prospects. The mechanism of K2S2O8 oxidation and graphiteexpansion under microwave irradiation was analyzed. In adition, flexible graphite foil papers preparedwith the obtained EG exhibit good electrical conductivity and thermal properties. The as preparedEG material shows an efficient adsorption of hydraulic oil and vegetable oil and excellent flame retardantperformance. This preparation method is green, low cost, and safe, and can be used for the efficient batchpreparation of EG.