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Lim, Kwang Soo,Baldoví,, José,J.,Jiang, ShangDa,Koo, Bong Ho,Kang, Dong Won,Lee, Woo Ram,Koh, Eui Kwan,Gaita-Ariñ,o, Alejandro,Coronado, Eugenio,Slota, Michael,Bogani, Lapo,Hong, Cha ACS AMERICAN CHEMICAL SOCIETY 2017 Inorganic Chemistry Vol.56 No.9
<P>Controlling the coordination sphere of lanthanoid complexes is a challenging critical step toward controlling their relaxation properties. Here we present the synthesis of hexacoordinated dysprosium single-molecule magnets, where tripodal ligands achieve a near-perfect octahedral coordination. We perform a complete experimental and theoretical investigation of their magnetic properties, including a full single-crystal magnetic anisotropy analysis. The combination of electrostatic and crystal-field computational tools (SIMPRE and CONDON codes) allows us to explain the static behavior of these systems in detail.</P>