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Burungale, V.V.,Satale, V.V.,More, A.J.,Sharma, K.K.K.,Kamble, A.S.,Kim, J.H.,Patil, P.S. Academic Press 2016 JOURNAL OF COLLOID AND INTERFACE SCIENCE - Vol.470 No.-
Exotic hierarchical rutile TiO<SUB>2</SUB> nanostructures are synthesized by surfactant free single step hydrothermal route. The effect of reaction temperature, ranging from 140<SUP>o</SUP>C to 200<SUP>o</SUP>C on the properties of the synthesized rutile-TiO<SUB>2</SUB> is investigated. The synthesized rutile-TiO<SUB>2</SUB> nanostructures are characterized using X-ray diffraction, X-ray photoelectron spectroscopy, Raman spectroscopy, UV-vis spectroscopy and scanning electron microscopy techniques. The deposited TiO<SUB>2</SUB> samples are found to be photoelectrochemically active and the best photoelectrochemical performance (0.95+/-0.05%) is obtained for the sample deposited at 180<SUP>o</SUP>C. A possible temperature dependent growth mechanism resulting in photochemically active TiO<SUB>2</SUB> nanostructure thin films is proposed.