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Sadaf Ul Hassan,Sadaf Ahmad,Muhammad Asim Farid,Sohail Nadeem,Zulfiqar Ali,Rashid Abro,Aysha Mohyuddin,Muhammad Shahid Nazir,Murid Hussain,박영권 한국공업화학회 2022 Journal of Industrial and Engineering Chemistry Vol.116 No.-
Hydrodesulfurization is a common but less effective technique to remove sulfur content of oils due to severe operating conditions of temperature, pressure and cost. Oxidative desulfurization(ODS) is preferable due to low cost and mild operating conditions. Coupling of the extractive catalytic desulfurization with the ODS give rise to extractive catalytic oxidative desulfurization(ECODS), a more promising for the elimination of sulfur contents of fuel oil. Herein we present by polyoxometalate based hybrids, [H2TPP][K5BVW11O40]•2CH3CN•2H2O (1), [H2TPP]2[K3BVW11O40]•CH3CN•3H2O (2), and [H2TPP]3[KBVW11O40]•2CH3CN (3) for efficient ECODS of hazardous model fuel. These were synthesized by facile method and characterized by elemental analysis, inductive couple plasma, powder X-ray diffraction analysis, thermo-gravimetric/differential thermal analysis, fourier transform infrared, and UV–visible analysis. These polyoxometalate based hybrids contain cations [H2TPP]2+(organic) and [BVW11O40]7−(inorganic) with stoichiometric ratios(i.e., 1:1, 2:1, 3:1). The stoichiometry of these hybrids was also established by Job’s analysis which agreed well with the results of TG-DTA and elemental analyses. Interestingly, an increase in catalytic efficiency is observed with increase of organic cations. The maximum ∼99.5 % conversion of dibenzothiophene at 60 °C after 2 h has been achieved with hybrid 3 which could be employed up to ten cycles without a significant decrease in efficiency.
Mutational Analysis of Prohibitin - A Highly Conserved Gene in Indian Female Breast Cancer Cases
Najm, Mohammad Zeeshan,Akhtar, Md. Salman,Ahmad, Istaq,Sadaf, Sadaf,Mallick, Mohd Nasar,Kausar, Mohd Adnan,Chattopadhyay, Shilpi,Ahad, Amjid,Zaidi, Shuaib,Husain, Syed Akhtar,Siddiqui, Waseem Ahmad Asian Pacific Journal of Cancer Prevention 2012 Asian Pacific journal of cancer prevention Vol.13 No.10
Prohibitin (PHB) is a chaperone protein which is highly conserved evolutionarily. It shows significant homology with the Drosophila cc gene which is considered important for development and differentiation of Drosophila melanogaster. Investigations have revealed an involvement of PHB in cellular proliferation and development, apoptosis, signal transduction, mitochondrial function and regulation of the estrogen and androgen receptors. Therefore, we conducted the present study to analyze mutations in the highly conserved region in Indian female breast cancer patients. Conventional PCR-SSCP and Automated DNA sequencing were performed with a total of 105 breast cancer samples along with adjacent normal tissue. Of the total, 14.2% (15/105) demonstrated a mutation status of prohibitin observed in our study population. We identified a novel missense mutation (Thr>Ser), a novel deletion of T nucleotide in an intron adjacent to intron-exon boundary and a previously determined missense mutation (Val>Ala). A statistically significant correlation was obtained which suggested that prohibitin may be associated with tumor development and/or progression of at least some proportion of breast cancers.
Entrenchment Effect and Audit Quality in Family Business of Pakistan
TAHIR, Safdar Husain,AKRAM, Sadaf,PERVEEN, Shahida,AHMAD, Gulzar,ULLAH, Muhammad Rizwan Korea Distribution Science Association 2020 The Journal of Asian Finance, Economics and Busine Vol.7 No.8
The purpose of this study is to test both the alignment theory and entertainment theory on family firms listed on the Pakistan Stock Exchange. To achieve these goals, we collected secondary data from 164 non-financial family firms in various sectors during 2014-18. These family firms are classified into two categories: family control firms and family owned firms. We take the audit fee and the audit quality as dependent variables while family control firms, family-owned firms, and family CEOs as independent variables. In addition, the study uses leverage, profit and export as control variables. To test the effect of the explanatory variables on the output variables, we use two econometric models, Ordinary Least Square and the Probit regression model. In addition, Huber Sandwich test is used to check the non-normality and heteroscedasticity of panel data. Contrary to the alignment effect, the study supports the entrenchment effect and advocates that family-controlled firms as well as family-owned firms are not conscientious regarding the selection of external auditors during their contracts with audit firms. They are less likely to pay high audit fees for good quality audit in Pakistan. Furthermore, the study shows a statistically significant and positive relationship between audit quality and audit fees.