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- 저자 : S. M. Abdelbasir (검색결과 1 건)
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S. M. Abdelbasir,S. M. El-Sheikh,M.M. Rashad,D.A. Rayan 대한금속·재료학회 2018 ELECTRONIC MATERIALS LETTERS Vol.14 No.4
Cuprous oxide Cu2Onanopowders were purposefully synthesised from waste electric cables (WECs) via a simple precipitationroute at room temperature using lactose as a reducing agent. In this regard, dimethyl sulfoxide (DMSO) was first appliedas an organic solvent for the dissolution of the cable insulating materials. Several parameters were investigated during dissolutionof WECs such as dissolution temperature, time and solid/liquid ratio to determine the dissolution percentage of theinsulating materials in DMSO. The morphology and the optical properties of the formed Cu2Oparticles were investigatedusing X-ray diffraction (XRD), field emission-scanning electron microscopy (FE-SEM), Fourier-transform infrared spectroscopyand UV–visible–near IR spectrophotometer. XRD data confirmed the presence of single crystalline phase of Cu2Onanoparticles. FE-SEM and TEM images revealed spherical, cubic and octahedral shapes with the various particle sizesranged from 16 to 57 nm depending on the synthesis conditions. A possible mechanism explaining the Cu2Onanostructuresformation was proposed. The band gap energies of the Cu2Onanostructures were estimated and the values were locatedbetween 1.5 and 2.08 eV. Photoluminescence spectroscopy analysis clearly showed a noticeably blue-shifted emission forthe synthesized samples compared to spectrum of the bulk. Eventually, magnetic properties of the synthesized nanoparticleshave been measured by vibrating sample magnetometer and the attained results implied that the synthesized particles areweakly ferromagnetic in nature at normal temperature.
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