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      • SCIESCOPUSKCI등재

        PREPARATION OF SUPPORTED PALLADIUM MEMBRANE AND SEPARATION OF HYDROGEN

        Morooka, Shigeharu,Kusakabe, Katsuki,Aoki, Kanna,Yokoyama, Shuichi 한국화학공학회 1996 Korean Journal of Chemical Engineering Vol.13 No.5

        Palladium acetate was sublimed at a reduced pressure at 400℃, carried into the macropores of the porous wall of an α-alumina support tube and was decomposed there. A thin palladium membrane which was thus formed showed a hydrogen permeance of 10^6 ㏖·m ²·s ¹·Pa ¹ and a hydrogen/nitrogen permselectivity higher than 1000. The membrane was stable against hydrogen embrittlement even when the permeation temperature was varied between 100 and 300℃, and it was stable to sulfur or chlorine. To test the ability of this system for the separation of hydrogen and deuterium. a palladium disk was used instead of the prepared membrane since a definite membrane thickness was necessary for calculation. When H₂ and D₂ permeated through the membrane independently, the H/D permselectivity was approximately 7 at 150-200℃ under a feed side pressure of 0.4 MPa and a permeate side pressure of 0.1 MPa. When a mixture of H₂ and D, was fed, the H/D permselectivity was reduced to 1.2-1.6.

      • KCI등재

        Seismic Performance Evaluation of a School Gymnasium Using Static Anlysis

        Morooka, Shigehiro,Tsuda, Seita,Ohsaki, Makoto 한국공간구조학회 2009 한국공간구조학회지 Vol.9 No.4

        학교체육관과 같은 소규모 공간구조물의 지진응답은 본래 지진동에 대한 동적응답을 시각이력해석에 의해 검증해야 하지만 통상은 정적해석에 의해 평가하고 있다. 본 연구에서는 학교 체육관의 내진성능평가를 가능하게 하는 정적해석의 진행수순을 나타내기로 한다. 지진하중은 2개의 성능 레벨 즉, 일본의 건축기준법에 정의되어 있는 레벨 1과 2에 대응하는 등가인 정적하중으로 근사한다. 또한, 재하 패턴으로서 고유모드형을 사용하는 것에 대한 중요성을 논의하고, 정적해석의 간단한 순서에 의해 최대연직방향가속도를 평가할수 있는 것을 나타낸다. 아울러, 레벨 2의 입력에 의한 정적해석은 동적해석으로 얻어진 응답치를 과소평가하지만, 일본의 중층구조에 사용되는 "극한내력계산법"에 근사한 등가선형차 기법에 의해 레벨 2의 입력에 대한 탄소성응답이 가능하다는 것을 나타내고자 한다. The seismic responses of small-scale spatial frames such as school gymnasiums are usually evaluated using static analysis, although time-history analysis should be carried out to fully incorporate the dynamic responses of the structures against seismic motions. In this study, advanced static analysis procedures arc presented for school gymnasiums that will improve the performance evaluation against seismic motions. The seismic loads are approximated by equivalent static loads corresponding to the two performance levels; i.e., Levels 1 and 2 defined by the Japanese building standard. The importance of utilizing the eigenmode in the load pattern is discussed. Simple static analysis procedures are presented for evaluation of maximum vertical acceleration. It is shown that the static analysis for Level 2 input significantly underestimates the responses by dynamic analysis; however, the inelastic responses for Level 2 are shown to be successfully evaluated using the equivalent linearization that is similar to the $^{\circ}$Dmethod based on calculation of limit strength$^{\circ}{\pm}$ for building frames in Japan.

      • KCI등재

        정적해석에 의한 학교 체육관의 내진 성능 평가

        Shigehiro Morooka,Seita Tsuda,Makoto Ohsaki 한국공간구조학회 2009 한국공간구조학회지 Vol.9 No.4

        The seismic responses of small-scale spatial frames such as school gymnasiums are usually evaluated using static analysis, although time-history analysis should be carried out to fully incorporate the dynamic responses of the structures against seismic motions. In this study, advanced static analysis procedures are presented for school gymnasiums that will improve the performance evaluation against seismic motions. The seismic loads are approximated by equivalent static loads corresponding to the two performance levels; i.e., Levels 1 and 2 defined by the Japanese building standard. The importance of utilizing the eigenmode in the load pattern is discussed. Simple static analysis procedures are presented for evaluation of maximum vertical acceleration. It is shown that the static analysis for Level 2 input significantly underestimates the responses by dynamic analysis; however, the inelastic responses for Level 2 are shown to be successfully evaluated using the equivalent linearization that is similar to the “method based on calculation of limit strength” for building frames in Japan. 학교체육관과 같은 소 규모 공간구조물의 지진응답은 본래 지진동에 대한 동적응답을 시각이력해석에 의해 검증해야 하지만 통상은 정적해석에 의해 평가하고 있다. 본 연구에서는 학교 체육관의 내진성능평가를 가능하게 하는 정적해석의 진행수순을 나타내기로 한다. 지진하중은 2개의 성능 레벨 즉, 일본의 건축기준법에 정의되어 있는 레벨 1과 2에 대응하는 등가인 정적하중으로 근사한다. 또한, 재하 패턴으로서 고유모드형을 사용하는 것에 대한 중요성을 논의하고, 정적해석의 간단한 순서에 의해 최대연직방향가속도를 평가할 수 있는 것을 나타낸다. 아울러, 레벨 2의 입력에 의한 정적해석은 동적해석으로 얻어진 응답치를 과소평가하지만, 일본의 중층구조에 사용되는 “극한내력계산법”에 근사한 등가선형화 기법에 의해 레벨 2의 입력에 대한 탄소성응답이 가능하다는 것을 나타내고자 한다.

      • SCIESCOPUSKCI등재

        RUMINAL AND POST-RUMINAL DIGESTlON AND NITROGEN BALANCE IN EARLY WEANED CALVES FED SOYBEAN MEAL AND HEATED SOYBEAN MEAL

        Obitsu, T.,Morooka, T.,Okubo, M.,Asahida, Y. Asian Australasian Association of Animal Productio 1995 Animal Bioscience Vol.8 No.1

        Two digestion trials were conducted to investigate the effect of feeding heated soybean meal (HSBM) on ruminal and post-ruminal digestion of organic matter (OM) and nitrogen (N), bacterial N flow to the duodenum and N balance in young calves weaned at 6 weeks of age. In trial 1, calves were fed concentrate diets containing soybean meal (SBM) or HSBM and hay mixed in the ratio of 6:4 to support daily weight gain of 0.5 kg. The same concentrate diets were used in trial 2, but the ratio of concentrate to hay was 7:3 to support body weight gain of 0.7 kg/d. Measurements were made 10 and 13 weeks of age in trial 1, and at 10 and 15 weeks in trial 2. Ruminal OM digestibility increased with advancing age in both trials. Ruminal OM digestion was not affected by the diets in trial 1, but it was greater for the SBM diet than for the HSBM diet at 10 weeks in trial 2. Net N loss from the rumen was lover for the HSBM diet than for the SBM diet in trial 1, but it was not affected by the diets in trial 2. Bacterial N flow to the duodenum, N digestion in the total digestive tract and N retention were not affected by the diets in either of the trials.

      • SCIESCOPUSKCI등재

        Development of A Microchannel Catalytic Reactor System

        Kusakade, Katsuki,Morooka, Shigeharu,Maeda, Hideaki 한국화학공학회 2001 Korean Journal of Chemical Engineering Vol.18 No.3

        The purpose of this article is to demonstrate the applicability of microreactors for use in catalytic reactions at elevated temperatures. Microchannels were fabricated on both sides of a silicon wafer by wet chemical etching after pattern transfer using a negative photoresist. The walls of the reactor channel were coated with a platinum layer, for use as a sample catalyst, by sputtering. A heating element was installed in the channel on the opposite surface of the reactor channel. The reactor channel was sealed gas-tight with a glass plate by using an anodic bonding technique. A small-scale palladium membrane was also prepared on the surface of a 50-㎛ thick copper film. In the membrane preparation, a negative photoresist was spin-coated and solidified to serve as a protective film. A palladium layer was then electrodeposited on the other uncovered surface. After the protective film was removed, the resist was again spin-coated on the copper surface, and a pattern of microslits was transferred by photolithography. After development, the microslits were electrolitically etched away, resulting in the formation of a palladium membrane as an assemblage of thin layers formed in the microslits. The integration of the microreactor and the membrane is currently under way.

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