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Fabrication of β-CoV3O8 nanorods embedded in graphene sheets and their application for electrochemical charge storage electrode

Jeong, Gyoung Hwa,Lee, Ilbok,Lee, Donghyun,Lee, Hea-Min,Baek, Seungmin,Kwon, O-Pil,Kumta, Prashant N,Yoon, Songhun,Kim, Sang-Wook IOP 2018 Nanotechnology Vol.29 No.19
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The fabrication of β-CoV3O8 nanorods embedded in graphene sheets and their application as electrochemical charge storage electrodes is reported. From the surfactant treatment of raw graphite, graphene was directly prepared and its nanocomposite with β-CoV3O8 nanorods distributed between graphene layers (β-CoV3O8-G) was synthesized by a hydrothermal method. When applied as an anode in lithium-ion batteries, the β-CoV3O8-G anode exhibits greatly improved charge and discharge capacities of 790 and 627 mAhаиаg−1, respectively, with unexpectedly high initial efficiency of 82%. The observed discharge capacity reflected that at least 3.7 mol of Li+ is selectively accumulated within the β-CoV3O8 phase (LixCoV3O8, xа>а3.7), indicative of significantly improved Li+ uptake when compared with aggregated β-CoV3O8 nanorods. Moreover, very distinct peak plateaus and greatly advanced cycling performance are observed, showing more improved Li+ storage within the β-CoV3O8 phase. As a supercapacitor electrode, moreover, our composite electrode exhibits very high peak pseudocapacitances of 2.71 Fаиаcm−2 and 433.65 Fаиаg−1 in the β-CoV3O8 phase with extremely stable cycling performance. This remarkably enhanced performance in the individual electrochemical charge storage electrodes is attributed to the novel phase formation of β-CoV3O8 and its optimized nanocomposite structure with graphene, which yield fast electrical conduction through graphene, easy accessibility of ions through the open multilayer nanosheet structure, and a relaxation space between the β-CoV3O8-G.
2
Understanding the Effects of Surface Finish on Diffusion Bonding of AZ31 Alloys

Matthew Criado,Abhijit Roy,John Ohodnicki,Nicholas Tondravi,Hannah Fischer,Alejandro Almarza,Howard A. Kuhn,Prashant N. Kumta 대한용접접합학회 2023 대한용접·접합학회지 Vol.41 No.5
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  KCI
  
  DBpia
Methods to optimize the diffusion bonding (DB) process while also creating lap joints were investigated using AZ31, the commercial Mg alloy, focusing primarily on studying the effects of varying conventional process parameters and more importantly, exploring the influence of surface roughness on creating an acceptable strong bond. The results indicate that when contact is made between surface areas of roughness (Ra > 0.2 ㎛) diffusion is facilitated at reduced process parameters of time and temperature. Furthermore, this early bond initiation combined with the optimized DB process parameters results in a stronger bond with strengths increasing by ~ 150% in comparison to the DB samples created with a smooth surface finish. Additionally, less than 20% total overall distortion is observed while preserving a uniform microstructure of consistent grain sizes in the material over the entire joining region compared with the parent material.